Method for producing hydrocarbon oil and system for producing hydrocarbon oil

Patent metadata

Field	Value
Publication number	US-9493714-B2
Application number	US-201113817182-A
Country	US
Kind code	B2
Filing date	Aug 12, 2011
Priority date	Aug 19, 2010
Publication date	Nov 15, 2016
Grant date	Nov 15, 2016

Abstract

Hydrocarbon oil obtained by Fischer-Tropsch (FT) synthesis reaction using a catalyst within a slurry bed reactor is fractionated into a distilled oil and a column bottom oil in a rectifying column, part of the column bottom oil is flowed into a first transfer line that connects a column bottom of the rectifying column to a hydrocracker, at least part of the column bottom oil is flowed into a second transfer line branched from the first transfer line and connected to the first transfer line downstream of the branching point, the amount of the catalyst fine powder to be captured is monitored while the catalyst fine powder in the column bottom oil that flows in the second transfer line are captured by a detachable filter provided in the second transfer line, and the column bottom oil is hydrocracked within the hydrocracker.

First claim

The invention claimed is:

1. A method for producing a hydrocarbon oil, comprising:
obtaining a hydrocarbon oil containing a catalyst fine powder derived from a catalyst by a Fischer-Tropsch synthesis reaction using a slurry bed reactor in which the catalyst is suspended in a liquid hydrocarbon;
fractionating the hydrocarbon oil into at least one distilled oil and a column bottom oil containing the catalyst fine powder using a rectifying column;
flowing at least part of the column bottom oil through a second transfer line to capture, using a detachable filter, the catalyst fine powder in the column bottom oil that is flowing through the second transfer line,
the second transfer line being branched from a branching point of a first transfer line, provided with the detachable filter at a halfway point, and connected to the first transfer line downstream of the branching point and
the first transfer line not having a filter between the branching point and the point where the second transfer line is connected to the first transfer line downstream of the branching point;
flowing the remaining column bottom oil through the first transfer line to transfer the column bottom oil to a hydrocracker in a transfer device comprising the first transfer line that connects a column bottom of the rectifying column to the hydrocracker;
monitoring an amount of the catalyst fine powder captured by the filter; and
hydrocracking the column bottom oil in the hydrocracker.

2. The method for producing a hydrocarbon oil according to claim 1 , wherein a ratio F 2 /F 1 of a mass flow rate F 2 of the column bottom oil to be transferred by the second transfer line to a mass flow rate F 1 of the column bottom oil to be transferred by the first transfer line is 0.01 to 0.2.

3. The method for producing a hydrocarbon oil according to claim 1 , wherein monitoring comprises measuring the amount of catalyst fine powder captured by the filter.

4. The method for producing a hydrocarbon oil according to claim 1 , wherein monitoring comprises calculating a difference in pressure before and after the filter, and estimating the amount of the catalyst fine powder captured by the filter based on the difference in pressure.

5. The method for producing a hydrocarbon oil according to claim 1 , wherein the first transfer line does not contain a filter for monitoring an amount of the catalyst fine powder.

Assignees

• Tasaka Kazuhiko
• Tanaka Yuichi
• Iwama Marie
• Japan Oil Gas & Metals Jogmec
• Inpex Corp
• Jx Nippon Oil & Energy Corp
• Japan Petroleum Exploration Co Ltd
• Cosmo Oil Co Ltd
• Nippon Steel & Sumikin Eng Co

Inventors

• Tasaka Kazuhiko
• Tanaka Yuichi
• Iwama Marie

Classifications

• Y02P30/20

  using bio-feedstock · CPC title

• C10G3/56

  suspended in the oil, e.g. slurries, ebullated beds · CPC title

• C10G31/00

  Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for (by distillation C10G7/00) · CPC title

• C10G2300/1022

  Fischer-Tropsch products · CPC title

• C10G47/00

  Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions (C10G15/00 takes precedence; destructive hydrogenation of non-melting solid carbonaceous or similar materials C10G1/06) · CPC title