Filtering distributor plate for supplying a fixed bed reactor having a co-current downflow of gas and liquid for the treatment of heavy clogging feeds

Patent metadata

Field	Value
Publication number	US-9480957-B2
Application number	US-201314050567-A
Country	US
Kind code	B2
Filing date	Oct 10, 2013
Priority date	Oct 10, 2012
Publication date	Nov 1, 2016
Grant date	Nov 1, 2016

Abstract

The present invention describes a distributor plate adapted to co-current downflow flows of gas and of liquid, more particularly in the “trickle” mode, said distributor plate integrating a filtration function separate from the distribution function.

First claim

The invention claimed is:

1. A fixed bed reactor with a co-current downflow gas-liquid flow comprising a distribution and filtration plate suitable for said gas-liquid flow, said fixed bed reactor optionally comprising a plurality of beds of catalyst staged along the reactor, each plate being positioned upstream of each catalytic bed, said plate comprising the following elements from top to bottom:
a perforated support ( 3 ) not covering the whole section of the reactor, but leaving free an annular zone ( 11 ) corresponding to 5% to 50% of the section of said reactor,
a filtration layer ( 4 ) supported by said perforated support ( 3 ),
a full plate ( 2 ) located at a distance of 50 mm to 150 mm with respect to the perforated support ( 3 ), comprising a plurality of substantially vertical distribution elements ( 5 ) crossing the filtration layer ( 4 ) and the full plate ( 2 ), these distribution elements being disposed in a rectangular or triangular pattern, said distribution elements ( 5 ) having a height of 200 mm to 400 mm, being open at their upper end to admit gas and comprising at least one row of holes located in the portion of said distribution elements which is comprised between the perforated support ( 3 ) and the full plate ( 2 ), in order to admit the liquid, and the gas-liquid mixture being evacuated by the lower end of said distribution element ( 5 ),
at least one high porosity dispersive element ( 7 ) located below the full plate ( 2 ) at a distance of 20 mm to 300 mm with respect to said full plate ( 2 ).

2. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 1 , in which each distribution and filtration plate has distribution elements ( 5 ) that are substantially vertical chimneys surrounded by full sleeves ( 8 ) over the portion of the height which corresponds to the depth of the filtration layer ( 4 ).

3. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 2 in which the pitch of the chimneys is 100 to 300 mm.

4. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 1 , in which the filtration layer ( 4 ) of the perforated support ( 3 ) is at least one layer of guard material particles with a height of 100 mm to 300 mm.

5. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 1 , in which the high porosity dispersive elements ( 7 ) located below the full plate ( 2 ) are disposed in a staggered manner and alternate between a distance of 150 mm and a distance of 250 mm below said full plate ( 2 ).

6. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 1 , in which a protective screen ( 6 ) for breaking the liquid jet entering the reactor is disposed above the filtration layer ( 4 ).

7. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 1 , in which the dispersive element ( 7 ) comprising an assembly of conical deflectors, each deflector being placed below a distribution element ( 5 ).

8. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 1 wherein annular zone ( 11 ) corresponds to 5% to 30% of the section of said reactor.

9. The fixed bed reactor with a co-current downflow gas-liquid flow according to claim 1 , wherein element ( 7 ) is located below the full plate ( 2 ) at a distance of 50 mm to 150 mm.

Assignees

• Ifp Energies Now

Inventors

• Bazer-Bachi Frederic
• Haroun Yacine
• Digne Mathieu

Classifications

• C10G49/002

  Apparatus for fixed bed hydrotreatment processes · CPC title

• B01J8/0278

  Feeding reactive fluids (for solid material B01J8/0015) · CPC title

• B01J8/0242 Primary

  the fluid flow within the bed being predominantly vertical · CPC title

• B01J8/0492

  Feeding reactive fluids (for solid material, see B01J8/0015) · CPC title

• B01J2208/025

  Two or more types of catalyst · CPC title