Age-hardening process featuring anomalous aging time

Patent metadata

Field	Value
Publication number	US-9469893-B2
Application number	US-201313903501-A
Country	US
Kind code	B2
Filing date	May 28, 2013
Priority date	Jul 16, 2010
Publication date	Oct 18, 2016
Grant date	Oct 18, 2016

Abstract

This document describes a process/strategy for age hardening nickel based alloys to create desirable properties with reduced energy expenditure. The inventive process introduces isolated atom nucleation sites to accelerate the nucleation rate by approximately 36 times, thereby permitting age hardening to occur in significantly less time and with significantly less energy expenditure.

First claim

The invention claimed is:

1. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging, comprising:
a. providing a metal alloy containing nickel, molybdenum, chromium, and rhenium;
b. wherein said rhenium comprises 3% to 10% of the total weight of said metal alloy;
c. wherein said nickel comprises 60% to 70% of the total weight of said metal alloy;
d. wherein said molybdenum comprises 20% to 30% of the total weight of said metal alloy;
e. wherein said chromium comprises 5% to 10% of the total weight of said metal alloy;
f. annealing said metal alloy; and
g. after said annealing step, subjecting said metal alloy to an age hardening process that forms long-range-ordered precipitates of the form Ni 2 Re.

2. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 1 , wherein said age hardening is conducted at a temperature in excess of 800 K.

3. A method, for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 1 , wherein said time interval used for said age hardening is less than fifteen minutes.

4. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 3 , wherein said time interval used for said age hardening is less than five minutes.

5. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 4 , wherein said age hardening is conducted at a temperature of about 873 K.

6. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 3 , wherein said age hardening is conducted at a temperature of about 873 K.

7. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 1 , wherein said age hardening process is continued for an interval of one minute.

8. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging, comprising:
a. providing a metal alloy containing nickel, molybdenum, chromium, and rhenium;
b. wherein said rhenium comprises to 10% of the total weight of said metal alloy;
c. wherein said nickel comprises 60% to 70% of the total weight of said metal alloy;
d. wherein said molybdenum comprises 20% to 30% of the total weight of said metal alloy;
e. wherein said chromium comprises 5% to 10% of the total weight of said metal alloy;
f. annealing said metal alloy at a temperature above 1200 K; and
g. after said annealing step, subjecting said metal alloy to an age hardening process that forms long-range-ordered precipitates of the form Ni 2 Re for a time interval of less than fifty minutes at a temperature above 800 K.

9. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 8 , wherein said age hardening is conducted at a temperature of about 873 K.

10. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of oven-aging as recited in claim 9 , wherein said time interval used for said age hardening is less than five minutes.

11. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging as recited in claim 8 , wherein said time interval used for said age hardening is less than five minutes.

Assignees

• Han Ke
• Mao Pingli
• Xin Yan
• Univ Florida State Res Found

Inventors

• Han Ke
• Mao Pingli
• Xin Yan

Classifications

• C22C19/057

  with the maximum Cr content being less 10% · CPC title

• C22F1/10 Primary

  of nickel or cobalt or alloys based thereon · CPC title