Flash vessel and method for operating same

Patent metadata

Field	Value
Publication number	US-9464341-B2
Application number	US-201214370882-A
Country	US
Kind code	B2
Filing date	Dec 27, 2012
Priority date	Jan 13, 2012
Publication date	Oct 11, 2016
Grant date	Oct 11, 2016

Abstract

A hydrostatic tower whose lower part communicates with a liquid phase space within a flash vessel, and whose upper part communicates with a gas phase space within the flash vessel is provided. A rising liquid level within the hydrostatic tower is detected by at least one maximum liquid level sensor provided at a position at the same level as a predetermined maximum liquid level within the liquid phase space. A dropping liquid level within the hydrostatic tower is detected by at least one minimum liquid level sensor provided at a position at the same level as a predetermined minimum liquid level within the liquid phase space.

First claim

The invention claimed is:

1. A flash vessel whose liquid level rises and drops considerably used in a high pressure acid leach step which includes leaching nickel oxide ore slurry under high temperature and pressure conditions by using an autoclave, and reducing the temperature and pressure of the slurry after leach to the ordinary temperature and ordinary pressure by using the flash vessel, comprising:
a hydrostatic tower whose lower part is coupled on a slurry outlet pipe between the connection position of the slurry outlet pipe and the flash vessel and the position of a slurry outlet valve, and whose upper part is coupled on a vapor outlet pipe;
at least one maximum liquid level sensor provided at a position at the same level as a maximum liquid level not causing inflow of the slurry into the vapor outlet pipe due to considerable rise and drop of the slurry liquid level within the liquid phase space of the flash vessel to detect a rising liquid level within the hydrostatic tower; and
at least one minimum liquid level sensor provided, at a position at the same level as a minimum liquid, level not causing inflow of vapor into the slurry outlet pipe due to considerable rise and drop of the slurry liquid level within the liquid phase space to detect a dropping liquid. level within the hydrostatic tower; and
a slurry outlet valve controlled opening and closing according to the detection output by the maximum liquid level sensor and the minimum liquid level sensor detecting the liquid level of the hydrostatic tower, opened when the maximum liquid level sensor detects a rising liquid level within the hydrostatic tower and closed when the minimum liquid level sensor detects a dropping liquid level within the hydrostatic tower.

2. The flash vessel according to claim 1 , wherein a diameter A of the hydrostatic tower lies in the range 1/100×B≦A≦⅕×B in comparison with a diameter B of the flash vessel.

3. A method for operating a flash vessel whose liquid level rises and drops considerably used in a high pressure acid leach step which includes nickel oxide ore slurry under high temperature and pressure conditions by using an autoclave, and reducing the temperature and pressure of the slurry after leach to the ordinary temperature and ordinary pressure by using the flash vessel, the method comprising:
detecting a liquid level within a hydrostatic tower whose lower part is coupled on a slurry outlet pipe between the connection position of the slurry outlet pipe and the flash vessel and the position of a slurry outlet valve, and whose upper part is coupled on a vapor outlet pipe;
by using at least one maximum liquid level sensor provided at a position at the same level as a maximum liquid level not causing inflow of the slurry into the vapor outlet pipe due to considerable rise and drop of the slurry liquid level within the liquid phase space of the flash vessel, and at least one minimum liquid level sensor provided at a position at the same level as a minimum liquid level not causing inflow of vapor into the slurry outlet pipe due to considerable rise and drop of the slurry liquid level within the liquid phase space; and
opening a slurry outlet valve provided on a slurry outlet pipe derived from the flash vessel when the maximum liquid level sensor detects a rising liquid level within the hydrostatic tower, and closing the slurry outlet valve when the minimum liquid level sensor detects a dropping liquid level within the hydrostatic tower.

Assignees

• Sumitomo Metal Mining Co

Inventors

• Matsubara Satoshi
• Nakai Osamu
• Kyoda Yoji
• Sakamoto Takashi

Classifications

• C22B23/043 Primary

  Sulfurated acids or salts thereof · CPC title

• B01J2219/00182

  controlling the level of reactants in the reactor vessel · CPC title

• B01J3/04

  Pressure vessels, e.g. autoclaves · CPC title

• B01J4/008

  Feed or outlet control devices · CPC title

• C22B3/08

  Sulfuric acid {, other sulfurated acids or salts thereof} · CPC title