Spectroscopic device

Patent metadata

Field	Value
Publication number	US-9459143-B2
Application number	US-201214117924-A
Country	US
Kind code	B2
Filing date	Jun 21, 2012
Priority date	Jun 24, 2011
Publication date	Oct 4, 2016
Grant date	Oct 4, 2016

Abstract

A spectroscopic device includes a lamp house accommodating a light source inside, a spectrometer configured to disperse light from the lamp house, a temperature measurement means for measuring a temperature of the spectrometer, a heating means for heating the spectrometer, a storage means and a control unit. The storage means stores the detection temperature of the temperature measurement means at a time when an optical axis is stable in the spectrometer in a state where the light source is illuminated. The control unit is configured to control operation of the heating means, and to cause the heating means to operate, when the light source is illuminated from a light-off state, until a detection temperature of the temperature measurement means reaches the detection temperature stored in the storage means.

First claim

The invention claimed is:

1. A spectroscopic device comprising:
a lamp house accommodating a light source inside;
a spectrometer positioned to receive light from the light source;
temperature measurement means provided on the spectrometer, for measuring a temperature of the spectrometer;
heating means provided on the spectrometer and configured separately from the lamp house, for heating the spectrometer;
storage means for storing a detection temperature of the temperature measurement means at a time a base line of a chromatogram is stable in a state where the light source is illuminated; and
a control unit configured to control an operation of the heating means, and to cause the heating means to operate, when the light source is illuminated from a light-off state, only until a detection temperature of the temperature measurement means reaches the detection temperature stored in the storage means.

2. The spectroscopic device according to claim 1 , further comprising:
a fan configured to cool the lamp house,
wherein the control unit keeps the fan stopped when the light source is illuminated from the light-off state, and causes the fan to operate at a predetermined number of revolutions after the detection temperature of the temperature measurement means has reached the detection temperature stored in the storage means.

3. The spectroscopic device according to claim 2 , comprising:
a plurality of sets of the temperature measurement means and the heating means for performing temperature measurement and heating of the spectrometer at different positions, said plurality of sets of the temperature measurement means and the heating means being provided on the spectrometer,
wherein the storage means stores, for each temperature measurement means, the detection temperature of the temperature measurement means at a time the optical axis is stable in the spectrometer, and
wherein the control unit causes the plurality of heating means to operate based on the detection temperatures of the corresponding temperature measurement means.

4. The spectroscopic device according to claim 3 ,
wherein the storage means stores, instead of the detection temperature, a time after the light source is illuminated from the light-off state until the detection temperature of the temperature measurement means reaches the detection temperature at a time the optical axis is stable in the spectrometer according to an operation of the heating means, and
wherein the control unit causes the heating means to operate, based on the time stored in the storage means.

5. The spectroscopic device according to claim 2 ,
wherein the storage means stores, instead of the detection temperature, a time after the light source is illuminated from the light-off state until the detection temperature of the temperature measurement means reaches the detection temperature at a time the optical axis is stable in the spectrometer according to an operation of the heating means, and
wherein the control unit causes the heating means to operate, based on the time stored in the storage means.

6. The spectroscopic device according to claim 1 , comprising:
a plurality of sets of the temperature measurement means and the heating means for performing temperature measurement and heating of the spectrometer at different positions, said plurality of sets of the temperature measurement means and the heating means being provided on the spectrometer,
wherein the storage means stores, for each temperature measurement means, the detection temperature of the temperature measurement means at a time the optical axis is stable in the spectrometer, and
wherein the control unit causes the plurality of heating means to operate based on the detection temperatures of the corresponding temperature measurement means.

7. The spectroscopic device according to claim 6 ,
wherein the storage means stores, instead of the detection temperature, a time after the light source is illuminated from the light-off state until the detection temperature of the temperature measurement means reaches the detection temperature at a time the optical axis is stable in the spectrometer according to an operation of the heating means, and
wherein the control unit causes the heating means to operate, based on the time stored in the storage means.

8. The spectroscopic device according to claim 1 ,
wherein the storage means stores, instead of the detection temperature, a time after the light source is illuminated from the light-off state until the detection temperature of the temperature measurement means reaches the detection temperature at a time the optical axis is stable in the spectrometer according to an operation of the heating means, and
wherein the control unit causes the heating means to operate, based on the time stored in the storage means.

Assignees

• Gunji Masahide
• Shimadzu Corp

Inventors

• Gunji Masahide

Classifications

• G01N30/74

  Optical detectors {(measurement of intensity, velocity, spectral content, polarisation, or phase of infrared, visible or ultraviolet light G01J)} · CPC title

• G01J3/42

  Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry (beam switching arrangements G01J3/08) · CPC title

• G01J3/18

  using diffraction elements, e.g. grating (gratings per se G02B) · CPC title

• G01N2201/0231

  Thermostating · CPC title

• G01J3/02 Primary

  Details · CPC title