Separation of liquid components from a mixture

Patent metadata

Field	Value
Publication number	US-9457296-B2
Application number	US-201113884277-A
Country	US
Kind code	B2
Filing date	Nov 10, 2011
Priority date	Nov 10, 2010
Publication date	Oct 4, 2016
Grant date	Oct 4, 2016

Abstract

Operation of an oil-water separator or other liquid mixture separator is monitored. The separator uses a vessel through which a mixture of different liquid components flows horizontally. A plurality of ultrasound transducers is provided on a wall of the vessel at different heights at a common stage along the direction of the horizontal flow. Ultrasound at a plurality of different ultrasound wavelengths is transmitted through the vessel between transducers and ultrasound arriving transducers is detected. Parameter values of a model are fitted to the detection. A model is used that relates height dependent properties of liquid in the vessel to properties of the detected ultrasound transmission between transceivers, the model comprising at least a fittable parameter of a height dependent droplet size distribution in a least a sub-range of a height of liquid in the vessel. The model relating the droplet size distribution to ultrasound wavelength dependence of the properties of ultrasound transmission. The measured droplet size distribution may be used to determine the route of ultrasound paths and to control demulsification measures.

First claim

The invention claimed is:

1. A method of monitoring operation of a liquid mixture separator, the separator comprising a vessel through which a mixture of different liquid components flows in a horizontal direction, the separator comprising a plurality of ultrasound transducers on a wall of the vessel at different heights at a common horizontal position along the horizontal direction, the method comprising
transmitting ultrasound through the vessel from at least first part of the transducers and detecting ultrasound arriving at at least a second part of the transducers for a plurality of ultrasound wavelengths, including detecting a combination of response signals measured for ultrasound ray paths at mutually different angles to the horizontal, and between transducers of the first part and transducers of the second part at mutually different heights;
fitting parameter values of a model that relates a parameter of a height dependent droplet size distribution to the detected combination of response signals.

2. A method according to claim 1 , comprising automatically controlling application of demulsification measures to the liquid mixture in the vessel dependent on a fitted value of the parameter of the height dependent droplet size distribution.

3. A method according to claim 2 , comprising selecting between applying different demulsification measures or different combinations of demulsification measures dependent on said fitted value of the parameter of the height dependent droplet size distribution.

4. A method according to claim 2 , comprising selecting an intensity of the demulsification measures dependent on said fitted value of the parameter of the height dependent droplet size distribution.

5. A method according to claim 2 , comprising selecting a height dependence of the demulsification measures dependent on said fitted value of the parameter of the height dependent droplet size distribution.

6. A method according to claim 2 , wherein said common horizontal position is located along the horizontal direction and upstream of a further horizontal position at which the demulsification measures are applied, feed-forward control being used to control the application of the demulsification measures.

7. A method according to claim 1 , wherein the parameter values of the model include at least one parameter defining a liquid component ratio gradient, between corresponding pure bodies of the different liquid components.

8. A method according to claim 7 , wherein model fitting comprises determining ultrasound ray paths with non-zero curvature dependent on the liquid component ratio gradient.

9. A method according to claim 7 , wherein the parameters of the model include at least one parameter defining a transition height between an oil droplet in water emulsion and a water droplet in oil emulsion, the model providing for a discontinuity in the ultrasound wavelength dependent transmission properties at said transition height.

10. The method of claim 7 , wherein the liquid component ratio gradient is an oil-water ratio gradient.

11. The method of claim 7 , wherein the pure bodies of the different liquid components are an oil body and a water body.

12. The method of claim 1 , wherein a space within the vessel for the liquid mixture is located between the first part of the transducers and the second part of the transducers.

13. The method of claim 1 , wherein the liquid mixture separator is an oil-water separator.

14. A liquid mixture separator, comprising
a separation vessel;
a plurality of ultrasound transducers on a wall of the vessel at different heights at a common horizontal position along a horizontal direction of flow;
an ultrasound measurement control module coupled to the transducers, configured to cause ultrasound at a plurality of wavelengths to be transmitted through the separation vessel, from a first part of the transducers and to cause a combination of response signals to be detected by a second part of the transducers, the combination of response signals being measured for ultrasound ray paths at mutually different angles to the horizontal, and between transducers of the first part and transducers of the second part at mutually different heights;
a signal processing module coupled to the transducers, the signal processing module being configured to fit parameter values of a model that relates a parameter of height dependent droplet size distribution to the detected combination of response signals.

15. A liquid mixture separator according to claim 14 , comprising
controllable emulsion reducer that is operational in the separation vessel and
a demulsification control module, the demulsification control module being configured to control the emulsion reducer dependent on a fitted value of said height dependent droplet size distribution.

16. A liquid mixture separator according to claim 15 , wherein said common horizontal position is located upstream of a further horizontal position along the horizontal direction wherein the emulsion reducer is operational.

17. A liquid mixture separator according to claim 15 , wherein the controllable emulsion reducer is configured to apply selectable ones or selectable combinations of emulsion reduction measures in the separation vessel, the demulsification control module being configured to control selection of the emulsion reduction measures dependent on the fitted value of said height dependent droplet size distribution.

18. A liquid mixture separator according to claim 15 , wherein the controllable emulsion reducer is configured to apply at least one emulsion reduction measure with a selectable height dependence in said vessel, the demulsification control module being configured to control selection of the height dependence dependent on the fitted value of said height dependent droplet size distribution.

19. A liquid mixture separator according to claim 14 , wherein the vessel has a rounded cross-section at said common horizontal position, the transducers being clamped onto an exterior wall of the vessel, at least part of the transducers being configured to transmit ultrasound at respective transmission angles through the vessel that are different from the horizontal direction of flow.

20. The liquid mixture separator of claim 14 , wherein a space within the vessel for the liquid mixture is located between the first part of the transducers and the second part of the transducers.

21. The liquid mixture separator of claim 14 , which is an oil-water separator.

Assignees

• Jansen Rik
• Volker Arno Willem Frederik
• Van Capel Peter
• Nederlandse Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek Tno

Inventors

• Jansen Rik
• Volker Arno Willem Frederik
• Van Capel Peter

Classifications

• C10G33/02

  with electrical or magnetic means · CPC title

• G01N29/4418

  with a model, e.g. best-fit, regression analysis · CPC title

• G01F23/2962

  Measuring transit time of reflected waves · CPC title

• G01N29/348

  with frequency characteristics, e.g. single frequency signals, chirp signals (measuring frequency of mechanical vibrations or acoustic waves in general G01H1/06, G01H3/04; measuring frequency or analysing frequency spectra G01R23/00) · CPC title

• B01D17/12 Primary

  Auxiliary equipment particularly adapted for use with liquid-separating apparatus, e.g. control circuits · CPC title