Flame photometric detector

Patent metadata

Field	Value
Publication number	US-9448177-B2
Application number	US-201213660273-A
Country	US
Kind code	B2
Filing date	Oct 25, 2012
Priority date	Oct 25, 2012
Publication date	Sep 20, 2016
Grant date	Sep 20, 2016

Abstract

A flame photometric detector (FPD) for use in a gas chromatography (GC) apparatus is described. The FPD has an emission block that is maintained in a first temperature range, and a transfer line that is maintained in a second temperature range that is greater than the first temperature range. The FPD is coupled to a light detector, such as a photomultiplier tube (PMT).

First claim

The invention claimed is:

1. An apparatus for receiving a gas chromatography column, the apparatus comprising:
a transfer line having a first end and a second end opposing the first end;
a heater block disposed around a first portion of the transfer line, the heater block comprising a heater configured to maintain the first portion of the transfer line at a first temperature range;
an emission block configured to receive the second end of the transfer line; and
a body tube substantially surrounding a second portion of the transfer line such that a gap is provided between the body tube and the second portion of the transfer line, the body tube mechanically and thermally coupled to the emission block, wherein the emission block and the body tube are maintained at a second temperature range that is lower than the first temperature range, and the second portion of the transfer line is maintained at the first temperature range.

2. An apparatus as claimed in claim 1 , wherein the heater is a first heater and the emission block comprises a second heater configured to maintain the emission block at the second temperature range.

3. An apparatus as claimed in claim 2 , further comprising a controller configured to maintain the second heater so that the emission block is maintained at the second temperature range.

4. An apparatus as claimed in claim 1 , wherein the body tube is brazed to the emission block.

5. An apparatus as claimed in claim 1 , further comprising a jet housing disposed around the second portion of the transfer line, wherein the jet housing is brazed to the transfer line.

6. An apparatus as claimed in claim 5 , wherein the body tube is brazed to the emission block at a first end of the body tube, and the body tube is brazed to the jet housing at a second end of the body tube.

7. An apparatus as claimed in claim 5 , further comprising a space between the jet housing and the transfer line, wherein the space is configured to receive a gas.

8. An apparatus as claimed in claim 5 , further comprising a space between the jet housing and the body tube.

9. An apparatus as claimed in claim 1 , wherein the body tube is made of metal or a metal alloy.

10. A flame photometric detector (FPD), comprising:
a transfer line having a first end and a second opposing end;
a heater block disposed around a first portion of the transfer line, the heater block comprising a heater configured to maintain the first portion of the transfer line at a first temperature range;
an emission block configured to receive the second opposing end of the transfer line;
a body tube substantially surrounding a second portion of the transfer line such that a gap is provided between the body tube and the second portion of the transfer line, the body tube mechanically and thermally coupled to the emission block; and
a photodetector coupled to the emission block for receiving light from the emission block, wherein the emission block and the body tube are maintained at a second temperature range that is lower than the first temperature range and the second portion of the transfer line is maintained at the first temperature range.

11. An FPD as claimed in claim 10 , wherein the heater is a first heater and the emission block comprises a second heater configured to maintain the emission block at the second temperature range.

12. An FPD as claimed in claim 11 , further comprising a controller configured to maintain the second heater so that the emission block is maintained at the second temperature range.

13. An FPD as claimed in claim 10 , wherein the body tube is brazed to the emission block.

14. An FPD as claimed in claim 10 , further comprising a jet housing disposed around the second portion of the transfer line, wherein the jet housing is brazed to the transfer line.

15. An FPD as claimed in claim 14 , wherein the body tube is brazed to the emission block at a first end of the body tube, and the body tube is brazed to the jet housing at a second end of the body tube.

16. An FPD as claimed in claim 14 , further comprising a space between the jet housing and the transfer line, wherein the space is configured to receive a gas.

17. An FPD as claimed in claim 14 , further comprising a space between the jet housing and the body tube.

18. An FPD as claimed in claim 10 , wherein the body tube is made of metal or a metal alloy.

Assignees

• Agilent Technologies Inc

Inventors

• Rhodes Robert P

Classifications

• H05B1/0247

  For chemical processes · CPC title

• G01N30/68

  Flame ionisation detectors · CPC title

• H05B3/40

  Heating elements having the shape of rods or tubes (H05B3/62, H05B3/68, H05B3/78 take precedence) · CPC title

• G01N21/72 Primary

  using flame burners · CPC title