Continuous processes for hydrolyzing hemicelluloses from lignocellulosic materials with cleaning system
US-2015354019-A1 · Dec 10, 2015 · US
US9422257B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9422257-B2 |
| Application number | US-201414771842-A |
| Country | US |
| Kind code | B2 |
| Filing date | Feb 25, 2014 |
| Priority date | Mar 14, 2013 |
| Publication date | Aug 23, 2016 |
| Grant date | Aug 23, 2016 |
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Disclosed is a process for making HMF′ or a derivative of HMF by dehydrating one or more hexose sugars in a reduced oxygen environment, in another, related aspect, a method for improving the stability and resistance to degradation of an HMF product Involves adding one or more antioxidants to the HMF product.
Opening claim text (preview).
What is claimed is: 1. A process for making hydroxymethylfurfural from an aqueous solution including one or more hexoses, comprising dehydrating the aqueous hexose solution through exposure to an acid in a reduced oxygen environment. 2. A process according to claim 1 , wherein an ester or ether derivative of hydroxymethylfurfural is formed by conducting the dehydration in the presence of an alcohol or a carboxylic acid, respectively. 3. A process according to either of claim 1 or 2 , wherein oxygen is displaced from the headspace of a reactor in which the dehydration takes place by sparging in another, inert gas. 4. A process according to claim 3 , comprising sparging nitrogen or carbon dioxide into the reactor.
Preparation from natural products · CPC title
Solutions {(composition of solutions A61K47/00)} · CPC title
not condensed with another ring, e.g. ranitidine, furosemide, bufetolol, muscarine · CPC title
Alcohols; Phenols; Salts thereof, e.g. glycerol; Polyethylene glycols [PEG]; Poloxamers; PEG/POE alkyl ethers · CPC title
Furfural · CPC title
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