Production method for hydrophilic modified polyrotaxane

US9409999B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-9409999-B2
Application numberUS-201114004849-A
CountryUS
Kind codeB2
Filing dateDec 5, 2011
Priority dateMar 14, 2011
Publication dateAug 9, 2016
Grant dateAug 9, 2016

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  1. Title

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Abstract

Official abstract text for this publication.

The present invention aims to provide a method of producing a hydrophilic modified polyrotaxane, which enables production of a hydrophilic modified polyrotaxane excellent in storage stability in an industrially advantageous way. The present invention provides a method of producing a hydrophilic modified polyrotaxane, comprising: a hydrophilic modification step of preparing a solution of a hydrophilic modified polyrotaxane by modifying all or part of hydroxy groups on a cyclodextrin of a polyrotaxane with hydrophilic modifying groups, the polyrotaxane containing the cyclodextrin, a polyethylene glycol included in the cavities of the cyclodextrin molecules in a skewered manner, and a capping group that is placed at each end of the polyethylene glycol and prevents dissociation of the cyclodextrin molecules from the polyethylene glycol; and a drying step in which the prepared solution of the hydrophilic modified polyrotaxane is formed into a thin film state and dried.

First claim

Opening claim text (preview).

The invention claimed is: 1. A method of producing a hydrophilic modified polyrotaxane, comprising: a hydrophilic modification step of preparing a solution of a hydrophilic modified polyrotaxane by modifying all or part of hydroxy groups on a cyclodextrin of a polyrotaxane with hydrophilic modifying groups, the polyrotaxane containing the cyclodextrin, a polyethylene glycol included in the cavities of the cyclodextrin molecules in a skewered manner, and a capping group that is placed at each end of the polyethylene glycol and prevents dissociation of the cyclodextrin molecules from the polyethylene glycol; and a drying step in which the prepared solution of the hydrophilic modified polyrotaxane is formed into a thin film state and dried, a thickness of a thin film formed being 0.1 to 2 mm. 2. The method of producing a hydrophilic modified polyrotaxane according to claim 1 , wherein the polyethylene glycol has a weight average molecular weight of 1,000 to 500,000. 3. The method of producing a hydrophilic modified polyrotaxane according to claim 1 , wherein the drying step is carried out at a drying temperature of 70° C. to 200° C. 4. The method of producing a hydrophilic modified polyrotaxane according to the claim 1 , wherein the pressure in the dryer system in the drying step is equal to or lower than an atmospheric pressure. 5. The method of producing a hydrophilic modified polyrotaxane according to the claim 1 , wherein a drying time in the drying step is two minutes or shorter.

Assignees

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Classifications

  • Inclusion compounds, i.e. host-guest compounds, e.g. polyrotaxanes · CPC title

  • cyclic · CPC title

  • Cyclodextrin; Derivatives thereof · CPC title

  • End-capping · CPC title

  • Manufacture of films or sheets · CPC title

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What does patent US9409999B2 cover?
The present invention aims to provide a method of producing a hydrophilic modified polyrotaxane, which enables production of a hydrophilic modified polyrotaxane excellent in storage stability in an industrially advantageous way. The present invention provides a method of producing a hydrophilic modified polyrotaxane, comprising: a hydrophilic modification step of preparing a solution of a hydro…
Who is the assignee on this patent?
Yamasaki Tomoaki, Okazaki Shinya, Okazaki Hiroki, and 5 more
What technology area does this patent fall under?
Primary CPC classification C08B37/0015. Mapped technology areas include Chemistry & Metallurgy.
When was this patent published?
Publication date Tue Aug 09 2016 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 8 related publications on this page (citations in our corpus or others sharing the same primary CPC).