High modulus, toughened one-component epoxy structural adhesives with high aspect ratio fillers
US-2024110085-A1 · Apr 4, 2024 · US
US9403185B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9403185-B2 |
| Application number | US-201214241118-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 27, 2012 |
| Priority date | Aug 31, 2011 |
| Publication date | Aug 2, 2016 |
| Grant date | Aug 2, 2016 |
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The invention relates to a process for the impregnation of air core reactors or parts of air core reactors and impregnated air core reactors or parts thereof obtainable by said process.
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The invention claimed is: 1. A process for the impregnation of an air core reactor or a part of an air core reactor comprising the following steps: i) providing an air core reactor or a part of an air core reactor, ii) applying an impregnation system to the air core reactor or the part of the air core reactor wherein said impregnation system comprises a) a component comprising one or more epoxy group(s), b) a flexibilizer selected from the group consisting of a polyoxyalkylene, a polyether-polyamine and a mixture thereof, c) dicyandiamide; and d) an accelerator selected from the group consisting of an imidazole, an imidazole derivative, a urea derivative and a mixture thereof, iii) curing the impregnated air core reactor or the impregnated part of the air core reactor. 2. The process according to claim 1 , wherein the part of the air core reactor is a coil. 3. The process according to claim 1 , wherein the a) component is a compound having an average epoxy functionality of at least two. 4. The process according to claim 3 , wherein the a) component is a polyglycidylether of a polyhydric alcohol. 5. The process according claim 1 , wherein the flexibilizer is a polypropylene glycol or polyethylene glycol. 6. The process according to claim 1 , wherein the flexibilizer is present in an amount ranging from 40 to 70 wt. %, based on the amount of the sum of components b), c) and d). 7. The process according to claim 1 , wherein the dicyandiamide is present in an amount ranging from 25 to 45 wt. %, based on the amount of the sum of components b), c) and d). 8. The process according to claim 1 , wherein the accelerator is present in an amount ranging from 5 to 25 wt. %, based on the amount of the sum of components b), c) and d). 9. The process according to claim 1 , wherein the weight ratio of component a) to the sum of components b), c) and d) ranges from 20:1 to 2:1. 10. The process according to claim 1 , wherein the impregnation system is applied to the air core reactor or the part of the air core reactor as a two component system of A) composition A comprising at least component a) and B) composition B comprising at least component b), c) and d). 11. The process according to claim 1 , wherein the curing in step iii) is carried out at a temperature higher than 120° C. 12. The process according to claim 1 wherein the impregnation is carried out as a trickle impregnation or a vacuum pressure impregnation. 13. An impregnated air core reactor or part of an air core reactor obtained by the process according to any of claim 1 .
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