Dye-labeled polymers and methods for preparing same
US-2024327655-A1 · Oct 3, 2024 · US
US9399652B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9399652-B2 |
| Application number | US-201414758110-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 23, 2014 |
| Priority date | Jan 24, 2013 |
| Publication date | Jul 26, 2016 |
| Grant date | Jul 26, 2016 |
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Methods and intermediates useful for making compounds of Formula (I) are described, including a general method of making an alpha, beta-diamino ketone by reacting an imine with a 2-amino-substituted 1,3-dicarbonyl in a Mannich addition reaction to produce said alpha,beta-diamino ketone.
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That which is claimed is: 1. A compound of Formula IX: wherein: R 8 is H, hydroxy, silyloxy, acyloxy, or alkoxy; and R 9 is —N(R c R d ), —OR c , or —SR c , where R c and R d are each independently selected alkyl, aryl, or heteroaryl, or R c and R d together form an alkylene bridge; and X is a protecting group. 2. A method of making a co…
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