Distribution tray for distributing a polyphasic mixture with inclined peripheral conduits

Patent metadata

Field	Value
Publication number	US-9381487-B2
Application number	US-201214347255-A
Country	US
Kind code	B2
Filing date	Sep 10, 2012
Priority date	Sep 30, 2011
Publication date	Jul 5, 2016
Grant date	Jul 5, 2016

Abstract

The present invention concerns a plate for distributing a polyphase mixture in a reactor operating in trickle bed mode constituted by at least one gas phase and at least one liquid phase, the plate ( 10 ) being located above a bed of catalytic particles, comprising a plurality of chimneys ( 3 ), characterized in that a portion of the chimneys of the plate located near to the wall of the chamber of the reactor, those termed the peripheral chimneys, have an upper portion which is inclined at an angle with respect to the vertical.
The invention also concerns the use of the plate in a reactor with a view to carrying out hydrotreatment, hydrogenation or oxidation reactions.

First claim

The invention claimed is:

1. A distributor plate ( 10 ) for distributing a polyphase mixture in a reactor terminating in a semi-spherical dome ( 2 ), the reactor having a wall, the distributor plate ( 10 ) to be located in an upper portion of the reactor above a bed of catalytic particles ( 30 ), said distributor plate comprising:
a plurality of chimneys ( 3 ) wherein each of said chimneys is provided with orifices ( 4 ) for passage of liquid distributed over the whole height (Hc) of each of said chimneys, and an orifice ( 5 ) for the passage of gas located at an upper end of each of said chimneys wherein the portion of the chimneys located at the periphery of the, referred to hereafter as peripheral chimneys, have their upper portion inclined by an angle alpha with respect to the vertical, said angle alpha having a value in the range 10° to 45° the inclination being approximately directed towards the center of the distributor plate, and, when positioned within the reactor, said peripheral chimneys are located at a distance (D 1 ) in the range 25 to 450 mm from the wall of the reactor.

2. The distributor plate according to claim 1 , in which said distance (D 1 ) is in the range 25 to 250 mm.

3. The distributor plate according to claim 1 , in which said angle alpha is in the range 10° to 30°.

4. The distributor plate according to claim 1 , in which said peripheral chimneys ( 3 ) are inclined starting from a distance (d) with respect to the base of the distributor plate ( 10 ) which is in the range 10% to 80% of the total height of the chimneys.

5. The distributor plate according to claim 1 , in which the peripheral chimneys and the portion of the chimneys positioned centrally on said distributor plate are separated by a pitch in the range 100 to 250 mm.

6. The distributor plate according to claim 1 , in which the plurality of chimneys have a height (Hc) in the range 100 to 500 mm.

7. A process for the hydrotreatment or hydrogenation of oil cuts containing C4 to C20 carbon atoms, said process comprising performing the process in a reactor having a distributor plate in accordance with claim 1 located in an upper portion of the reactor above a bed of catalytic particles ( 30 ), and said process functioning in trickle bed mode, using a dispersed liquid phase having a surface velocity of less than 1.5 cm, and a gas phase which is the continuous phase.

8. The distributor plate according to claim 1 , in which said peripheral chimneys ( 3 ) are inclined starting from a distance (d) with respect to the base of the distributor plate ( 10 ) which is in the range 50% to 80% of the total height of the chimneys.

9. The distributor plate according to claim 1 , in which the peripheral chimneys and the portion of the chimneys positioned centrally on said distributor plate are separated by a pitch in the range 100 to 200 mm.

10. The distributor plate according to claim 1 , in which the plurality of chimneys have a height (Hc) in the range 200 to 350 mm.

11. A reactor and distributor plate comprising:
a vertical reactor wall ( 1 ) and an upper semi-spherical dome ( 2 ),
a distributor plate positioned ( 10 ) in an upper portion of the reactor above a bed of catalytic particles ( 30 ),
said distributor plate having a plurality of chimneys ( 3 ) wherein each of said chimneys is provided with orifices ( 4 ) for passage of liquid distributed over the whole height (Hc) of each of said chimneys, and an orifice ( 5 ) for the passage of gas located at an upper end of each of said chimneys,
wherein the portion of the chimneys located at the periphery of the plate, referred to hereafter as peripheral chimneys, have their upper portion inclined by an angle alpha with respect to the vertical, said angle alpha having a value in the range 10° to 45°, the inclination being directed towards the center of the reactor, and, when positioned within the reactor, said peripheral chimneys are located at a distance (D 1 ) in the range 25 to 450 mm from said wall of said reactor.

12. The reactor and distributor plate according to claim 11 , in which said distance (D 1 ) is in the range 25 to 250 mm.

13. The reactor and distributor plate according to claim 11 , in which said angle alpha is in the range 10° to 30°.

14. The reactor and distributor plate according to claim 11 , in which said peripheral chimneys ( 3 ) are inclined starting from a distance (d) with respect to the base of the distributor plate ( 10 ) which is in the range 10% to 80% of the total height of the chimneys.

15. The reactor and distributor plate according to claim 11 , in which the peripheral chimneys and the portion of the chimneys positioned centrally on said distributor plate are separated by a pitch in the range 100 to 250 mm.

16. The reactor and distributor plate according to claim 11 , in which the plurality of chimneys have a height (Hc) in the range 100 to 500 mm.

17. The reactor and distributor plate according to claim 11 , in which said peripheral chimneys ( 3 ) are inclined starting from a distance (d) with respect to the base of the distributor plate ( 10 ) which is in the range 50% to 80% of the total height of the chimneys.

18. The reactor and distributor plate according to claim 11 , in which the peripheral chimneys and the portion of the chimneys positioned centrally on said distributor plate are separated by a pitch in the range 100 to 200 mm.

19. The reactor and distributor plate according to claim 11 , in which the plurality of chimneys have a height (Hc) in the range 200 to 350 mm.

Assignees

• Bazer-Bachi Frederic
• Augier Frederic
• Haroun Yacine
• Boyer Christophe
• IFP Energies Nouvelles

Inventors

• Bazer-Bachi Frederic
• Augier Frederic
• Haroun Yacine
• Boyer Christophe

Classifications

• B01J2219/00761

  Details of the reactor · CPC title

• C10G49/002

  Apparatus for fixed bed hydrotreatment processes · CPC title

• B01J8/0278

  Feeding reactive fluids (for solid material B01J8/0015) · CPC title

• B01J8/0492 Primary

  Feeding reactive fluids (for solid material, see B01J8/0015) · CPC title

• C10G2300/202

  Heteroatoms content, i.e. S, N, O, P · CPC title