Plasma device for production of metal powder

Patent metadata

Field	Value
Publication number	US-9375789-B2
Application number	US-201214359837-A
Country	US
Kind code	B2
Filing date	Nov 8, 2012
Priority date	Dec 6, 2011
Publication date	Jun 28, 2016
Grant date	Jun 28, 2016

Abstract

A plasma device for production of metal powder includes a reaction vessel, a plasma torch, a carrier gas supply unit and a cooling tube. A metal starting material is supplied to the vessel. The torch produces plasma between the torch and the metal starting material to evaporate the metal starting material and produce a metal vapor. The supply unit supplies into the vessel a carrier gas for carrying the metal vapor. The cooling tube is provided with indirect and direct cooling sections and cools the metal vapor transferred from the vessel to produce the metal powder. The metal vapor and/or the metal powder are indirectly cooled in the indirect cooling section and directly cooled in the direct cooling section. A projection and/or a recess are disposed at least on a part of an inner wall of the indirect cooling section.

First claim

The invention claimed is:

1. A plasma device for production of metal powder, comprising:
a reaction vessel to which a metal starting material is supplied;
a plasma torch which produces plasma between the plasma torch and the metal starting material in the reaction vessel so as to evaporate the metal starting material and produce a metal vapor;
a carrier gas supply unit which supplies into the reaction vessel a carrier gas for carrying the metal vapor; and
a cooling tube which cools the metal vapor transferred from the reaction vessel with the carrier gas so as to produce the metal powder, wherein
the cooling tube is provided with: an indirect cooling section where the metal vapor transferred from the reaction vessel with the carrier gas and/or the metal powder are indirectly cooled; and a direct cooling section where the metal vapor and/or the metal powder are directly cooled, the direct cooling section being continuous with the indirect cooling section, and
at least on a part of an inner wall of the indirect cooling section, a projection and/or a recess are disposed.

2. The plasma device for production of metal powder according to claim 1 , wherein the projection and/or the recess are disposed on the inner wall on an upstream side from a position where a metal nucleus starts to be precipitated in the indirect cooling section.

3. The plasma device for production of metal powder according to claim 1 , wherein a plurality of the projections and/or a plurality of the recesses are disposed on the inner wall in the indirect cooling section.

4. The plasma device for production of metal powder according to claim 3 , wherein the plurality of the projections and/or the plurality of the recesses are disposed on the inner wall in the indirect cooling section spirally in a longitudinal direction of the cooling tube.

5. The plasma device for production of metal powder according to claim 1 , wherein
the indirect cooling section is a section where the metal vapor and/or the metal powder are cooled by cooling a periphery of the cooling tube with a cooling fluid without making the cooling fluid directly contact the metal vapor and/or the metal powder, and
the direct cooling section is a section where the metal vapor and/or the metal powder are cooled by making a cooling fluid directly contact the metal vapor and/or the metal powder.

6. A method for producing metal powder, comprising the steps of:
supplying the metal starting material to the reaction vessel of the plasma device for production of metal powder according to claim 1 ;
producing the plasma between the plasma torch and the metal starting material in the reaction vessel so as to evaporate the metal starting material and produce the metal vapor; and
indirectly cooling the metal vapor transferred from the reaction vessel with the carrier gas and/or the metal powder in the indirect cooling section of the cooling tube and thereafter directly cooling the metal vapor and/or the metal powder in the direct cooling section of the cooling tube, wherein
in the step of cooling, a mixed gas composed of the carrier gas and the metal vapor is stirred with the existence of the projection and/or the recess, which are disposed at least on the part of the inner wall of the indirect cooling section.

Assignees

• Shoei Chemical Ind Co

Inventors

• Shimizu Fumiyuki
• Maekawa Masayuki
• Kawaguchi Shusaku

Classifications

• B22F9/14

  using electric discharge · CPC title

• B01J19/088

  giving rise to electric discharges (for heating purposes H05B7/00; for the production of ozone C01B13/11, H01T19/00) · CPC title

• H05B7/18

  Heating by arc discharge · CPC title

• B01J2219/0879

  Solid · CPC title

• B01J2219/0871

  Heating or cooling of the reactor · CPC title