Manufacture of coated particulate detergents

Patent metadata

Field	Value
Publication number	US-9365811-B2
Application number	US-201113878440-A
Country	US
Kind code	B2
Filing date	Aug 10, 2011
Priority date	Oct 14, 2010
Publication date	Jun 14, 2016
Grant date	Jun 14, 2016

Abstract

A process to manufacture large coated detergent particles having perpendicular dimensions x, y and z, wherein x is from 0.2 to 2 mm, y is from 2.5 to 8 mm, and z is from 2.5 to 8 mm the particles being substantially the same shape and size as one another and the uncoated core particles comprising at least 50 wt % of soluble surfactant, the process comprising the steps of suspending uncoated core particles in a fluidized bed and spraying onto the core particles an aqueous slurry of sodium carbonate in admixture with 0.6 to 3 wt % sodium carboxy methyl cellulose and drying to form the coated particles.

First claim

The invention claimed is:

1. A process to manufacture coated detergent particles having a core and a coating, the coated detergent particles having perpendicular dimensions x, y and z, wherein x is from 0.2 to 2 mm, y is from 2.5 to 8 mm, and z is from 2.5 to 8 mm, and the uncoated core particles comprising at least 50 wt % of a soluble surfactant, the process comprising the steps of suspending uncoated core particles in a fluidised bed and spraying onto the core particles an aqueous slurry in which the slurry is sprayed at a temperature of at least 35° C., the aqueous slurry comprising: sodium carbonate in admixture with 0.6 to 3 wt % sodium carboxy methyl cellulose and drying to form the coated particles.

2. A process according to claim 1 in which the aqueous slurry comprises 45 to 60 wt % sodium carbonate.

3. A process according to claim 1 in which the maximum particle size of the slurry is at most 50 microns.

4. A process according to claim 1 in which the slurry is milled prior to spraying.

5. A process according to claim 1 in which the spraying is done by means of at least one spray head.

6. A process according to claim 5 in which the at Beast one spray head is immersed in the fluidised surfactant particles.

7. A process according to claim 1 in which the slurry is sprayed at a temperature of at least 45° C.

8. A process according to claim 1 in which the fluidising air temperature lies in the range 35 to 150° C.

9. A process according to claim 1 in which the ratio of slurry addition rate to air flow rate is in the range 30 to 350 m 3 air per 1 kg slurry spray.

10. A process to coat particles of extruded soluble surfactant comprising the steps of fluidising the particles of extruded soluble surfactant by means of an air current and then, while the particles of extruded soluble surfactant are in a fluidised state, spraying onto the particles of extruded soluble surfactant an aqueous slurry at a temperature of at least 35° C., the aqueous slurry comprising at least 33 wt % sodium carbonate and from 0.6 to 3 wt % of sodium carboxymethyl cellulose, the size of the sodium carbonate particles in the suspension is less than or equal to 50 microns.

11. A process according to claim 10 in which the slurry comprises up to 60 wt % sodium carbonate, optionally in admixture with other soluble or insoluble inorganic materials.

12. A process according to claim 1 in which the slurry comprises at most 5 wt % surfactant.

13. A process according to claim 1 in which the surfactant comprises a blend of linear alkyl benzene sulphonate (LAS) and ethoxylated alcohol nonionic surfactant.

14. A process according to claim 1 in which the slurry further comprises silicate.

Assignees

• Bonsall Judith Maria
• Moore Philip Ronald
• Conopco Inc

Inventors

• Bonsall Judith Maria
• Moore Philip Ronald

Classifications

• C11D3/10

  Carbonates {; Bicarbonates} · CPC title

• C11D3/225

  etherified, e.g. CMC · CPC title

• C11D11/0088

  the liquefied ingredients being sprayed or adsorbed onto solid particles · CPC title

• C11D17/06

  Powder; Flakes; Free-flowing mixtures; Sheets · CPC title

• C11D17/0039 Primary

  Coated compositions or coated components in the compositions, (micro)capsules · CPC title