Method for preparing a porous fluoropolymer and preparing an article of same
US-9452372-B2 · Sep 27, 2016 · US
US9364775B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9364775-B2 |
| Application number | US-201113880934-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 2, 2011 |
| Priority date | Nov 4, 2010 |
| Publication date | Jun 14, 2016 |
| Grant date | Jun 14, 2016 |
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Official abstract text for this publication.
A method of forming a filter element is disclosed comprising introducing a mixture into a feeder, the mixture comprising a plurality of susceptor particles and a plurality of polymeric binder particles. The mixture is advanced through the feeder and into a die comprising an excitation portion where eddy currents are induced in the susceptor particles by subjecting the mixture to a high-frequency electromagnetic field, the eddy currents being sufficient to elevate the temperature of the susceptor particles to cause adjacent polymeric binder particles to be heated to at least a softening point. The susceptor particles bind with the heated polymeric binder particles in the die to form a coherent mass. The coherent mass is advanced out of the die and cooled to form the filter element.
Opening claim text (preview).
What is claimed is: 1. A method of forming a filter element comprising: introducing a mixture into a feeder, the mixture comprising a plurality of activated carbon susceptor particles and a plurality of polymeric binder particles; advancing the mixture through the feeder and into a die, the die comprising an excitation portion; while advancing the mixture through the excitation portion, inducing eddy currents in the activated carbon susceptor particles by subjecting the mixture to a high-frequency electromagnetic field, the eddy currents being sufficient to elevate the temperature of the activated carbon susceptor particles to cause adjacent polymeric binder particles to be heated to at least a softening point; binding the activated carbon susceptor particles with the heated polymeric binder particles in the die to form a coherent mass; advancing the coherent mass out of the die; and cooling the coherent mass to form the filter element. 2. The method of claim 1 wherein the die further comprises a variable aperture portion following the excitation portion, the method further comprising: advancing the mixture through the variable aperture portion. 3. The method of claim 2 comprising setting an aperture of the variable aperture portion to regulate an extrusion profile of the coherent mass. 4. The method of claim 1 wherein the excitation portion of the die comprises a heating tube through which the mixture advances while being subjected to the high-frequency electromagnetic field, the heating tube comprising an electrically insulating material. 5. The method of claim 1 wherein the feeder does not cause compression of the mixture. 6. The method of claim 1 wherein the feeder comprises a feeder shaft, the feeder shaft comprising an auger portion and a core pin portion extending beyond the auger portion into the die; the method comprising rotating the auger portion to advance the mixture through the feeder; and the core pin forming an internal profile of the coherent mass such that the coherent mass is tubular. 7. The method of claim 6 further comprising not rotating the core pin portion. 8. The method of claim 6 wherein the core pin portion comprises an electrically insulating material. 9. The method of claim 1 wherein the feeder comprises a feeder exit positioned adjacent the die, the method comprising disrupting the mixture by radial expansion near the feeder exit to reduce any flow patterns established while advancing the mixture through the feeder. 10. The method of claim 9 wherein disrupting the mixture comprises allowing the mixture to expand radially outwardly upon leaving the feeder exit. 11. The method of claim 9 wherein disrupting the mixture comprises allowing the mixture to expand radially inwardly upon leaving the feeder exit. 12. The method of claim 10 wherein the feeder exit comprises a feeder exit diameter and the die comprises a die entrance portion; wherein the die entrance portion tapers outwardly from the feeder exit diameter. 13. The method of claim 11 wherein the feeder comprises a feeder shaft, the feeder shaft comprising an auger portion terminating near the feeder exit and a core pin portion extending beyond the auger portion into the die, the auger portion comprising an auger minor diameter; wherein the core pin portion tapers inwardly from the auger minor diameter. 14. The method of claim 3 wherein setting the aperture comprises inflating or deflating one or more bladders surrounding the heated mixture. 15. The method of claim 3 wherein setting the aperture comprises positioning a forming tube surrounding the heated mixture. 16. The method of claim 15 wherein the forming tube comprises a plurality of leaves surrounding the heated mixture, wherein setting the aperture comprises positioning the plurality of leaves surrounding the heated mixture. 17. The method of claim 15 wherein positioning the forming tube comprises actuating one or more actuators connected to the forming tube. 18. The method of claim 17 wherein one or more actuators comprises an inflatable bladder. 19. The method of claim 1 wherein the high-frequency electromagnetic field oscillates in a range from about 500 kHz to about 30 MHz. 20. The method of claim 1 wherein no heat is provided to the mixture while in the feeder. 21. The method of claim 1 wherein no cooling is provided to the mixture while in the feeder. 22. The method of claim 1 wherein the polymeric binder particles comprise ultra high molecular weight polyethylene. 23. The method of claim 1 wherein binding the activated carbon susceptor particles with the heated polymeric binder particles comprises sintering the mixture such that a coherent mass is formed but polymeric binder does not coat the susceptor particles. 24. The method of claim 3 further comprising forming a plurality of depressions in the extrusion profile as the coherent mass advances through the variable aperture portion. 25. The method of claim 6 wherein an induction heater is positioned circumferentially surrounding the core pin. 26. The method of claim 9 wherein disrupting the mixture comprises allowing the mixture to expand radially outwardly upon leaving the feeder exit and allowing the mixture to expand radially inwardly upon leaving the feeder exit. 27. The method of claim 15 wherein the forming tube surrounds the heated mixture and the forming tube surrounds a core pin.
Density, e.g. per unit length or area · CPC title
using force fields, e.g. gravity or electrical fields (B29C48/9165 takes precedence) · CPC title
Filters {(optical filters B29L2011/0066, sieves or screens B29L2031/737)} · CPC title
Permeability to liquids; Adsorption · CPC title
with annular openings, e.g. for forming tubular articles · CPC title
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