Film growing method
US-2015368779-A1 · Dec 24, 2015 · US
US9347126B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9347126-B2 |
| Application number | US-201313801478-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 13, 2013 |
| Priority date | Jan 20, 2012 |
| Publication date | May 24, 2016 |
| Grant date | May 24, 2016 |
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A process of fabricating a thermal barrier coating is disclosed. The process includes cold spraying a substrate with a feedstock to form a thermal barrier coating and concurrently oxidizing one or more of the substrate, the feedstock, and the thermal barrier coating. The cold spraying is in a region having an oxygen concentration of at least 10%. In another embodiment, the process includes heating a feedstock with a laser and cold spraying a substrate with the feedstock to form a thermal barrier coating. At least a portion of the feedstock is retained in the thermal barrier coating. In another embodiment, the process of fabricating a thermal barrier coating includes heating a substrate with a laser and cold spraying the substrate with a feedstock to form a thermal barrier coating.
Opening claim text (preview).
What is claimed is: 1. A process of fabricating a thermal barrier coating, the process comprising: cold spraying a substrate with a feedstock to form a thermal barrier coating on the substrate; and concurrently oxidizing one or more of the substrate, the feedstock, and the thermal barrier coating; wherein the cold spraying is in a region above the substrate having an oxygen concentration of at least 10%. 2. The process of claim 1 , wherein the oxygen concentration is provided by a process gas. 3. The process of claim 2 , wherein the process gas is air. 4. The process of claim 1 , wherein the oxygen concentration is provided by an inlet gas. 5. The process of claim 1 , wherein the oxygen concentration is above about 50%. 6. The process of claim 1 , wherein the oxygen concentration is above about 70%. 7. The process of claim 1 , wherein an oxide concentration is increased by an increase in the oxygen concentration. 8. The process of claim 1 , further comprising oxidizing at least a portion of the thermal barrier coating. 9. The process of claim 8 , wherein the oxidizing at least a portion of the thermal barrier coating includes baking in an oxygen containing atmosphere. 10. The process of claim 8 , wherein the oxidizing at least a portion of the thermal barrier coating includes chemical treatment. 11. The process of claim 1 , wherein the feedstock comprises mica. 12. The process of claim 11 , wherein a decomposition of the mica forms porosity in the thermal barrier coating. 13. The process of claim 1 , wherein the thermal barrier coating has graded porosity. 14. The process of claim 1 , wherein the feedstock further comprises a homogenous mixture of ceramic particles and a binder. 15. The process of claim 14 , wherein the ceramic particles comprise a material selected from the group consisting of 68.9 wt % Yb 2 O 3 , balance ZrO 2 ; high Y 55 wt %, balance ZrO 2 ; and combinations thereof. 16. The process of claim 14 , wherein the ceramic particles comprise a material selected from the group consisting of 30.5 wt % Yb 2 O 3 , balance ZrO 2 ; 24.8 wt % La 2 O 3 , balance ZrO 2 ; and combinations thereof. 17. The process of claim 1 , further comprising heating the feedstock prior to the cold spraying. 18. The process of claim 1 , further comprising heating the substrate prior to the cold spraying. 19. The process of claim 1 , further comprising heating the feedstock with a laser. 20. The process of claim 1 , further comprising heating the substrate with a laser.
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