Device and method for preprocessing metallic magnesium

Patent metadata

Field	Value
Publication number	US-9340851-B2
Application number	US-201414348703-A
Country	US
Kind code	B2
Filing date	Jan 21, 2014
Priority date	Dec 31, 2013
Publication date	May 17, 2016
Grant date	May 17, 2016

Abstract

Provided are a device and a method for preprocessing metallic magnesium. The device includes a chamber, a heating device mounted in the chamber, a gas inlet port mounted on the chamber, and a gas evacuation port mounted on the chamber. The gas inlet port is connected to external inert gas supply equipment for supplying an inert gas into the chamber. The gas evacuation port is connected to an external vacuum evacuation device to evacuate the chamber to vacuum. The heating device functions to heat metallic magnesium having an oxidized surface so as to sublimate a layer of magnesium oxide formed on the surface of the metallic magnesium in a vacuum environment to thereby obtain pure metallic magnesium.

First claim

What is claimed is:

1. A metallic magnesium preprocessing device, comprising: a chamber, a heating device mounted in the chamber, a gas inlet port mounted on the chamber, and a gas evacuation port mounted on the chamber, the gas inlet port being adapted to be connected to and in communication with an external inert gas supply equipment for supplying an inert gas into the chamber, the gas evacuation port being adapted to be connected to and in communication with an external vacuum evacuation device to evacuate the chamber to vacuum, the heating device heating metallic magnesium having an oxidized surface so as to sublimate a layer of magnesium oxide formed on the surface of the metallic magnesium in a vacuum environment to thereby obtain pure metallic magnesium; and further comprising an oxygen sensor arranged in the chamber and a vacuum gauge arranged in the chamber, the oxygen sensor detecting oxygen content inside the chamber, the vacuum gauge detecting pressure inside the chamber.

2. The metallic magnesium preprocessing device as claimed in claim 1 , wherein the gas inlet port is provided with a gas inlet valve for controlling opening and closing of the gas inlet port and the gas evacuation port is provided with a gas evacuation valve for controlling opening and closing of the gas evacuation port.

3. The metallic magnesium preprocessing device as claimed in claim 2 further comprising a control device, which controls actuation and de-actuation of the gas inlet valve and the gas evacuation valve.

4. The metallic magnesium preprocessing device as claimed in claim 3 , wherein the heating device comprises a base, a heating coil arranged on the base, and a cover mounted on the base and located outside and around the heating coil, the heating coil being formed by winding an electric heating wire of an iron chromium aluminum alloy or a nickel chromium alloy, the base and the cover being both made of metals, the heating device being controlled by the control device as to whether to carry out a heating operation.

5. The metallic magnesium preprocessing device as claimed in claim 4 , wherein the cover receives a temperature transducer mounted therein to detect a temperature of the heating device.

6. The metallic magnesium preprocessing device as claimed in claim 3 , wherein the control device is mounted on the chamber.

7. The metallic magnesium preprocessing device as claimed in claim 1 , wherein the chamber comprises a lighting device mounted therein and the chamber has a sidewall in which a transparent window is formed for observation a melting condition of the surface-oxidized metallic magnesium in the chamber.

8. The metallic magnesium preprocessing device as claimed in claim 1 further comprising a lining attachment-prevention board removably mounted inside the chamber.

9. A metallic magnesium preprocessing device, comprising: a chamber, a heating device mounted in the chamber, a gas inlet port mounted on the chamber, and a gas evacuation port mounted on the chamber, the gas inlet port being adapted to be connected to and in communication with an external inert gas supply equipment for supplying an inert gas into the chamber, the gas evacuation port being adapted to be connected to and in communication with an external vacuum evacuation device to evacuate the chamber to vacuum, the heating device heating metallic magnesium having an oxidized surface so as to sublimate a layer of magnesium oxide formed on the surface of the metallic magnesium in a vacuum environment to thereby obtain pure metallic magnesium;
wherein the gas inlet port is provided with a gas inlet valve for controlling opening and closing of the gas inlet port and the gas evacuation port is provided with a gas evacuation valve for controlling opening and closing of the gas evacuation port;
further comprising a control device, which controls actuation and de-actuation of the gas inlet valve and the gas evacuation valve;
further comprising an oxygen sensor arranged in the chamber and a vacuum gauge arranged in the chamber, the oxygen sensor detecting oxygen content inside the chamber, the vacuum gauge detecting pressure inside the chamber; and
wherein the heating device comprises a base, a heating coil arranged on the base, and a cover mounted on the base and located outside and around the heating coil, the heating coil being formed by winding an electric heating wire of an iron chromium aluminum alloy or a nickel chromium alloy, the base and the cover being both made of metals, the heating device being controlled by the control device as to whether to carry out a heating operation.

10. The metallic magnesium preprocessing device as claimed in claim 9 , wherein the cover receives a temperature transducer mounted therein to detect a temperature of the heating device.

11. The metallic magnesium preprocessing device as claimed in claim 9 , wherein the chamber comprises a lighting device mounted therein and the chamber has a sidewall in which a transparent window is formed for observation a melting condition of the surface-oxidized metallic magnesium in the chamber.

12. The metallic magnesium preprocessing device as claimed in claim 9 further comprising a lining attachment-prevention board removably mounted inside the chamber.

13. The metallic magnesium preprocessing device as claimed in claim 9 , wherein the control device is mounted on the chamber.

14. A method for preprocessing metallic magnesium, comprising the following steps:
(1) providing a preprocessing device, wherein the preprocessing device comprises: a chamber, a heating device mounted in the chamber, a gas inlet port mounted on the chamber, and a gas evacuation port mounted on the chamber, the gas inlet port being connected to and in communication with an external inert gas supply equipment, the gas evacuation port being connected to and in communication with an external vacuum evacuation device;
(2) placing surface-oxidized metallic magnesium in a crucible and placing the crucible on the heating device;
(3) evacuating interior of the chamber to vacuum through the gas evacuation port;
(4) introducing an inert gas into the chamber through the gas inlet port;
(5) repeating steps (3) and (4) until oxygen content inside the chamber becomes less than 1 ppm;
(6) evacuating the interior of the chamber to vacuum through the gas evacuation port so as to make an internal pressure of the chamber less than or equal to 10 −4 Pa;
(7) using the heating device to heat up the surface-oxidized metallic magnesium so as to completely sublimate magnesium oxide; and
(8) conducting cooling and then obtaining pure metallic magnesium;
wherein the gas inlet port is provided with a gas inlet valve for controlling opening and closing of the gas inlet port and the gas evacuation port is provided with a gas evacuation valve for controlling opening and closing of the gas evacuation port;
wherein the preprocessing device further comprises a control device, which controls actuation and de-actuation of the gas inlet valve and the gas evacuation valve;
wherein the preprocessing device further comprises an oxygen sensor arranged in the chamber and a vacuum gauge arranged in the chamber, the oxygen sensor detecting oxygen content inside the chamber, the vacuum gauge detecting pressure inside the chamber;
wherein the heating device comprises a base, a heating coil arranged on the base, and a cover mounted on the base and located outside and around the heating coil, the heating coil being formed by winding an electric heating wire of an iron chromium aluminum alloy or a nickel chromium alloy, the base and the cover being both made of metals, the heating

Assignees

• Shenzhen China Star Optoelect
• Shenzhen China Star Optoelect

Inventors

• Zou Qinghua
• Wu Tsungyuan
• Zhang Xindi

Classifications

• C22B9/05

  Refining by treating with gases, e.g. gas flushing {also refining by means of a material generating gas in situ} · CPC title

• F27D21/0014

  Devices for monitoring temperature · CPC title

• F27B5/06

  Details, accessories or equipment specially adapted for furnaces of these types · CPC title

• F27D2019/0012

  Monitoring the composition of the atmosphere or of one of their components · CPC title

• C22B4/02

  Light metals {(C22B4/005 takes precedence)} · CPC title