Carbon block filter

Patent metadata

Field	Value
Publication number	US-9339747-B2
Application number	US-200913124130-A
Country	US
Kind code	B2
Filing date	Sep 21, 2009
Priority date	Oct 17, 2008
Publication date	May 17, 2016
Grant date	May 17, 2016

Abstract

The present invention relates to a process for making metal impregnated bound Carbon block filters. In particular the present invention to a process for preparing a moulded Carbon block filter impregnated with a metal selected from Silver, Copper or Zinc, with relatively low level of variation in metal content across the blocks, relatively lower deviation from the theoretical metal content, and where the leach-rate of metal from the block during use is relatively low.

First claim

What is claimed is:

1. A process comprising:
(i) adding activated carbon particles to an aqueous solution of: (i) a salt of silver, zinc or copper and (ii) ammonium hydroxide to form an aqueous mix;
(ii) mixing the aqueous mix with a binder having a Melt Flow Rate less than 1 g/10 minutes to form a mixture;
(iii) adding the mixture to a mould;
(iv) heating the mould to a temperature in the range of 150° C. to 350° C. for 90 minutes to 300 minutes and applying sufficient pressure to form a carbon block filter having uniform metal impregnation;
wherein the uniform metal impregnation of the carbon block filter is measured as a deviation of an average metal content of the carbon block filter from a theoretical metal content of the carbon block filter of 5% or less; and,

(v) removing the carbon block filter from the mould.

2. The process of claim 1 , wherein the salt is at least one of silver nitrate, zinc nitrate and copper nitrate.

3. The process of claim 2 , wherein of the salt is silver nitrate and a concentration of the silver nitrate in the aqueous solution is 0.01 to 10 wt % of the aqueous solution.

4. The process of claim 1 , wherein a concentration of ammonium hydroxide in the aqueous solution is 0.1 to 10 wt % of the aqueous solution.

5. The process of claim 1 , wherein a ratio of the ammonium hydroxide to the salt of the silver, zinc or copper is 1:2 to 1:10.

6. The process of claim 1 , wherein a ratio of the activated carbon particles to the aqueous solution of the salt is 1:0.4 to 1:2.

7. The process of claim 1 , wherein the average metal content of the carbon block filter is equal to the theoretical metal content of the carbon block filter.

Assignees

• Dave Parthiv Ripudaman
• Mukherjee Debasis
• Srivastava Madalasa
• Conopco Inc

Inventors

• Dave Parthiv Ripudaman
• Mukherjee Debasis
• Srivastava Madalasa

Classifications

• B01D2239/0464

  Impregnants · CPC title

• B01D2239/1291

  Other parameters · CPC title

• B01D2239/10

  Filtering material manufacturing · CPC title

• B01D39/2062 Primary

  Bonded, e.g. activated carbon blocks · CPC title

• B01D2239/086

  Binders between particles or fibres · CPC title