NMR detection probe

Patent metadata

Field	Value
Publication number	US-9335389-B2
Application number	US-201313971957-A
Country	US
Kind code	B2
Filing date	Aug 21, 2013
Priority date	Aug 23, 2012
Publication date	May 10, 2016
Grant date	May 10, 2016

Abstract

A cooled NMR detection probe including a detection coil and an internal structure ( 65 ) mounted in a vacuum vessel ( 58 ) includes a radiation shield assembly ( 68 ), a connecting member ( 74 ), and a heat exchanger ( 80 ). The internal structure ( 65 ) is secured to the vacuum vessel ( 58 ) by a holding member ( 66 ). If the internal structure shrinks during cooling, the position of an upper portion of the first heat exchanger ( 80 ) hardly varies, thus suppressing displacement of a core module ( 54 ).

First claim

The invention claimed is:

1. An NMR detection probe comprising:
a vacuum vessel inserted in a static magnetic field generator and extending along a central axis, the vacuum vessel having a bottom at a bottom height;
an internal structure mounted in the vacuum vessel and having a detection coil for detecting an NMR signal emanating from a sample and a cooling source for cooling the coil; and
a holding member for holding the internal structure to the vacuum vessel above the bottom height of the vacuum vessel as viewed along the central axis, said holding member having an elongated portion extending along the central axis between the vacuum vessel and the internal structure.

2. The NMR detection probe as set forth in claim 1 , wherein said holding member includes an outer end portion secured to said vacuum vessel, an inner end portion supporting said internal structure, and an intermediate portion located between the outer end portion and the inner end portion and including said elongated portion.

3. The NMR detection probe as set forth in claim 2 , wherein said elongated portion is made up of a plurality of links spaced from each other.

4. The NMR detection probe as set forth in claim 2 , wherein said internal structure has a radiation shield that extends along an inner surface of said vacuum vessel in an up-and-down direction and blocking infrared radiation, and wherein said inner end portion holds the radiation shield, which in turn supports said cooling source.

5. The NMR detection probe as set forth in claim 4 , wherein a connecting member made of a heat insulating material is mounted at an intermediate position of said radiation shield that is lower than a position at which said inner end portion is held, and wherein said cooling source is supported by said radiation shield via the connecting member.

6. The NMR detection probe as set forth in claim 1 , wherein said internal structure depends from and is secured to an upper portion of said vacuum vessel via said holding member.

7. The NMR detection probe as set forth in claim 1 , further comprising restriction means for restricting horizontal motion of a lower portion of said internal structure.

8. The NMR detection probe as set forth in claim 7 , wherein said restriction means includes a first member extending downward from said cooling source and a second member engaging with the first member and restricting horizontal motion of the first member while permitting sliding motion of the first member along the central axis.

9. The NMR detection probe as set forth in claim 1 , wherein a detection module having said detection coil is held to said cooling source via a hard heat conductor, and wherein the detection module is isolated from said vacuum vessel via a vacuum insulating layer.

Assignees

• Univ Kyoto
• Jeol Resonance Inc

Inventors

• Takegoshi Kiyonori
• Mizuno Takashi

Classifications

• G01R33/30 Primary

  Sample handling arrangements, e.g. sample cells, spinning mechanisms · CPC title

• G01R33/3403

  Means for cooling of the RF coils, e.g. a refrigerator or a cooling vessel specially adapted for housing an RF coil · CPC title

• G01R33/34 Primary

  Constructional details, e.g. resonators {, specially adapted to MR} · CPC title

• G01R33/307

  specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer · CPC title

• G01R33/31

  Temperature control thereof · CPC title