Compositions comprising estolide compounds and methods of making and using the same
US-9840606-B2 · Dec 12, 2017 · US
US9327342B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9327342-B2 |
| Application number | US-201113027327-A |
| Country | US |
| Kind code | B2 |
| Filing date | Feb 15, 2011 |
| Priority date | Jun 14, 2010 |
| Publication date | May 3, 2016 |
| Grant date | May 3, 2016 |
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Forge lubrication processes are disclosed. A solid lubricant sheet is placed between a workpiece and a die in a forging apparatus. Force is applied to the workpiece with the die to plastically deform the workpiece. The solid lubricant sheet decreases the shear friction factor for the forging system and reduces the incidence of die-locking.
Opening claim text (preview).
What is claimed is: 1. A forge lubrication process comprising: positioning a solid graphite sheet into a formed die cavity, in contact with a working surface of a die, and between a workpiece and the die in a closed-die forging apparatus, the solid graphite sheet comprising a pre-formed non-planar shape that matches a non-planar contour of at least a region of the die, and the workpiece comprising one of titanium, a titanium alloy, zirconium, and a zirconium alloy, wherein the solid graphite sheet comprises the pre-formed non-planar shape before contacting the working surface of the die; and applying force to the workpiece to plastically deform the workpiece; wherein the workpiece is at a temperature greater than 1000° F. during the deformation, and a shear friction factor between the die and the workpiece during deformation is less than 0.50. 2. The process of claim 1 , wherein the workpiece is at a temperature in the range of 1000° F. to 1600° F. during deformation, and the shear friction factor between the dies and the workpiece during deformation is in the range of 0.09 to 0.20. 3. The process of claim 1 , wherein positioning the solid graphite sheet between the workpiece and the die in the closed-die forging apparatus comprises: inserting the solid graphite sheet into the formed die cavity in the closed-die forging apparatus, wherein the pre-formed shape of the solid graphite sheet matches a contour of at least a region of the die in the die cavity; and inserting the workpiece into the die cavity and onto the solid graphite sheet; wherein the solid graphite sheet is positioned between a bottom surface of the workpiece and an upper surface of the die in the die cavity. 4. The process of claim 1 , wherein the workpiece is plastically deformed in one of a near-net-shape forging process and a net-shape forging process. 5. The process of claim 1 , wherein the solid graphite sheet is rigid and maintains the pre-formed non-planar shape before being positioned in the die. 6. The process of claim 1 , wherein the solid graphite sheet does not comprise a bonding agent. 7. The process of claim 1 , wherein the solid graphite sheet consists of graphite and residual impurities. 8. The process of claim 1 , wherein the positioning of the solid graphite sheet does not comprise adhering the sheet to the working surface of the die. 9. A forge lubrication process comprising: positioning a solid lubricant sheet into a formed die cavity, in contact with a working surface of a die, and between a workpiece and the die in a closed-die forging apparatus, the solid lubricant sheet comprising a pre-formed non-planar shape that matches a non-planar contour of at least a region of the die, wherein the solid lubricant sheet comprises the pre-formed non-planar shape before contacting the working surface of the die; and applying force to the workpiece with the die to plastically deform the workpiece. 10. The process of claim 9 , wherein the shear friction factor between the dies and the workpiece during forging is less than 0.50. 11. The process of claim 9 , wherein the shear friction factor between the dies and the workpiece during forging is less than 0.20. 12. The process of claim 9 , wherein the solid lubricant sheet comprises a solid-state lubricant material selected from the group consisting of graphite, molybdenum disulfide, tungsten disulfide, and boron nitride. 13. The process of claim 9 , wherein the solid lubricant sheet is a solid graphite sheet. 14. The process of claim 9 , wherein positioning the solid lubricant sheet between the workpiece and the die in a closed-die forging apparatus comprises: inserting the solid lubricant sheet into the formed die cavity in the die, wherein the pre-formed shape of the solid lubricant sheet matches a contour of at least a region of the die in the die cavity; and inserting the workpiece into the die cavity and onto the solid lubricant sheet; wherein the solid lubricant sheet is positioned between a bottom surface of the workpiece and an upper surface of the die in the die cavity. 15. The process of claim 9 , wherein positioning the solid lubricant sheet between the workpiece and the die in the closed-die forging apparatus comprises: inserting the pre-formed non-planar shaped solid lubricant sheet into the formed die cavity in the closed-die forging apparatus, wherein the pre-formed non-planar shaped solid lubricant sheet comprises a pre-formed non-planar shape that matches a contour of at least a region of a lower die in the die cavity; and inserting the workpiece into the die cavity and onto the pre-formed non-planar shaped solid lubricant sheet; and further comprising: positioning a second solid lubricant sheet between a top surface of the workpiece and a lower surface of an upper die in the closed-die forging apparatus. 16. The process of claim 9 , wherein positioning the solid lubricant sheet between the workpiece and the die in the closed-die forging apparatus comprises: inserting the pre-formed non-planar shaped solid lubricant sheet into the formed die cavity in the closed-die forging apparatus, wherein the pre-formed non-planar shaped solid lubricant sheet comprises a pre-formed shape that matches a contour of at least a region of a lower die in the die cavity; and inserting the workpiece into the die cavity and onto the pre-formed non-planar shaped solid lubricant sheet; and further comprising: positioning a second solid lubricant sheet on a top surface of the workpiece in the die cavity. 17. The process of claim 9 , wherein positioning the solid lubricant sheet between the workpiece and the die in the closed-die forging apparatus comprises: inserting the pre-formed non-planar shaped solid lubricant sheet into the formed die cavity in the closed-die forging apparatus, wherein the pre-formed non-planar shaped solid lubricant sheet comprises a pre-formed shape that matches a contour of at least a region of a lower die in the die cavity; and inserting the workpiece into the die cavity and onto the pre-formed non-planar shaped solid lubricant sheet; and further comprising: positioning a second solid lubricant sheet on a lower surface of an upper die in the closed-die forging apparatus, wherein the second solid lubricant sheet comprises a pre-formed shape that matches a contour of at least a region of the upper die. 18. The process of claim 9 , wherein applying force to the workpiece with the die to plastically deform the workpiece occurs while the workpiece is at a temperature greater than 1000° F. 19. The process of claim 9 , wherein applying force to the workpiece with the die to plastically deform the workpiece occurs while the workpiece is at a temperature in the range of 1000° F. to 1600° F. 20. The process of claim 9 , wherein the workpiece is plastically deformed in a near-net-shape forging process. 21. The process of claim 9 , wherein the workpiece is plastically deformed in a net-shape forging process. 22. The process of claim 9 , wherein the workpiece comprises a titanium alloy. 23. The process of claim 9 , wherein the workpiece comprises a zirconium alloy. 24. The process of claim 9 , further comprising removing residual solid lubricant from the workpiece after the workpiece is plastically deformed. 25. The process of claim 9 , wherein the solid lubricant sheet is rigid and maintains the pre-formed non-planar shape before being positioned in
Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure · CPC title
Solids · CPC title
of specific metals · CPC title
without essential removal of material {, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding}; Punching metal · CPC title
Groups 4 or 14 · CPC title
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