Use of aluminum nitride to obtain temperature measurements in a high temperature and high radiation environment

Patent metadata

Field	Value
Publication number	US-9322720-B2
Application number	US-201414186244-A
Country	US
Kind code	B2
Filing date	Feb 21, 2014
Priority date	Feb 25, 2013
Publication date	Apr 26, 2016
Grant date	Apr 26, 2016

Abstract

An aluminum nitride piezoelectric ultrasonic transducer successfully operates at temperatures of up to 1000° C. and fast (>1 MeV) neutron fluencies of more than 10 18 n/cm 2 . The transducer comprises a transparent, nitrogen rich aluminum nitride (AlN) crystal wafer that is coupled to an aluminum cylinder for pulse-echo measurements. The transducer has the capability to measure in situ gamma heating within the core of a nuclear reactor.

First claim

We claim:

1. A temperature sensing apparatus for testing a nuclear reactor, the temperature sensing apparatus comprising:
an electrode;
a piezoelectric wafer connected electrically to the electrode, the piezoelectric wafer withstanding neutron fluencies of 1018 n/cm 2 or more;
a sensor block that thermally expands with a change in temperature in the nuclear reactor, the sensor block being connected to the piezoelectric wafer;
a compression mechanism; and
a transducer housing and a cap, both the transducer housing and the cap enclosing the piezoelectric wafer, the electrode, the sensor block, and the compression mechanism;
wherein the transducer housing and the cap are electrically grounded, and the sensor block and the compression mechanism are connected electrically to the transducer housing and the cap; and
wherein the apparatus is configured to measure within the nuclear reactor a time an ultrasonic pulse takes to travel from a first end of the sensor block to a second end of the sensor block and back to the first end of the sensor block.

2. The apparatus according to claim 1 , wherein the apparatus is configured to measure via electrical pulses the time the ultrasonic pulse takes to travel from the first end of the sensor block to the second end of the sensor block and back to the first end of the sensor block.

3. The apparatus according to claim 1 , wherein the piezoelectric wafer withstands temperatures of 1000° C. or more.

4. The apparatus according to claim 1 , wherein the piezoelectric wafer comprises a pyroelectric piezoelectric material.

5. The apparatus according to claim 4 , wherein the piezoelectric wafer comprises aluminum nitride.

6. The apparatus according to claim 4 , wherein the piezoelectric wafer comprises a 5.3 mm diameter single crystal z-cut of aluminum nitride.

7. The apparatus according to claim 4 , wherein the piezoelectric wafer comprises transparent nitrogen rich aluminum nitride.

8. The apparatus according to claim 1 , wherein the piezoelectric wafer comprises a ferroelectric piezoelectric material.

9. The apparatus according to claim 4 , further comprising an adhesive that attaches the piezoelectric wafer and a backing to the sensor block, the backing providing electrical conduction from the electrode to the piezoelectric wafer.

10. The apparatus according to claim 9 , wherein the backing is a carbon-carbon backing.

11. The apparatus according to claim 4 , wherein the sensor block is an aluminum cylinder, the aluminum cylinder being about 15 mm in diameter and about 65 mm in length.

12. The apparatus according to claim 1 , further comprising insulators that electrically isolate the electrode from the transducer housing and the cap.

13. A method for testing a nuclear reactor comprising:
(a) placing a temperature sensing apparatus within the nuclear reactor, the apparatus comprising an electrode; a piezoelectric wafer connected electrically to the electrode, the piezoelectric wafer withstanding neutron fluencies of 1018 n/cm 2 or more; and a sensor block that thermally expands with a change in temperature in the nuclear reactor, the sensor block being connected to the piezoelectric wafer;
(b) applying an electrical input pulse to the piezoelectric wafer through the electrode;
(c) creating at a first end of the sensor block an ultrasonic pulse based on the electrical input pulse, wherein the ultrasonic pulse propagates along the sensor block to a second end of the sensor block and is reflected back to the first end of the sensor block;
(d) receiving at the electrode an electrical output pulse based on the reflected pulse;
(e) measuring a time between the applying the electrical input pulse and the receiving the electrical output pulse; and
(f) calculating a temperature in the nuclear reactor.

14. The method according to claim 13 , wherein the piezoelectric wafer withstands temperatures of 1000° C. or more.

15. The method according to claim 13 , wherein the piezoelectric wafer comprises a pyroelectric piezoelectric material.

16. The method according to claim 15 , wherein the piezoelectric wafer comprises aluminum nitride.

17. The method according to claim 15 , wherein the piezoelectric wafer comprises a 5.3 mm diameter single crystal z-cut of aluminum nitride.

18. The method according to claim 15 , wherein the piezoelectric wafer comprises transparent nitrogen rich aluminum nitride.

19. The method according to claim 13 , wherein the piezoelectric wafer comprises a ferroelectric piezoelectric material.

Assignees

• Us Energy
• Us Dept Energy

Inventors

• Wernsman Bernard R
• Blasi Raymond J
• Tittman Bernhard R
• Parks David A

Classifications

• G01K11/22 Primary

  using measurement of acoustic effects · CPC title

• G01N29/245

  Ceramic probes, e.g. lead zirconate titanate [PZT] probes · CPC title

• G01K11/24 Primary

  of the velocity of propagation of sound · CPC title

• G01K13/00

  Thermometers specially adapted for specific purposes · CPC title