Method for manufacturing ceramic honeycomb structure

Patent metadata

Field	Value
Publication number	US-9321189-B1
Application number	US-201313873933-A
Country	US
Kind code	B1
Filing date	Apr 30, 2013
Priority date	Mar 15, 2013
Publication date	Apr 26, 2016
Grant date	Apr 26, 2016

Abstract

A method for manufacturing a ceramic honeycomb structure includes kneading inorganic particles and binder ingredient such that raw material paste including the inorganic particles and binder ingredient is prepared, forming a body made of the raw material paste and having a honeycomb structure such that the body has the honeycomb structure having multiple through-holes extending in the longitudinal direction of the body and multiple partitions formed between the through-holes, degreasing of the body including heating the body in atmosphere maintaining oxygen concentration of 0.2% or less in the first heating and heating the body in atmosphere having oxygen concentration which is higher than the oxygen concentration of the first heating in the second heating such that a degreased body having the honeycomb structure is formed, and sintering the degreased body having the honeycomb structure such that a ceramic body having the honeycomb structure is formed.

First claim

What is claimed is:

1. A method for manufacturing a ceramic honeycomb structure, comprising:
kneading inorganic particles and a binder ingredient such that a raw material paste comprising the inorganic particles and the binder ingredient is prepared;
forming a body comprising the raw material paste and having a honeycomb structure such that the body has the honeycomb structure having a plurality of through-holes extending in a longitudinal direction of the body and a plurality of partition portions formed between the through-holes;
degreasing the body comprising heating the body comprising the raw material paste in an atmosphere maintaining an oxygen concentration of 0.2% or less in a first heating and heating the body comprising the raw material paste in an atmosphere having an oxygen concentration which is higher than the oxygen concentration of the first heating in a second heating such that a degreased body having the honeycomb structure is formed; and
sintering the degreased body having the honeycomb structure at a temperature in a range of 1350° C. to 1650° C. such that a ceramic body having the honeycomb structure is formed,
wherein the degreasing comprises maintaining a surface temperature of the body in a range of 400° C. to 600° C. in the first heating and the second heating.

2. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the body is heated in the first heating such that a surface temperature of the body reaches a temperature in a range of 450° C.˜600° C.

3. The method for manufacturing a ceramic honeycomb structure according to claim 2 , wherein the first heating of the body includes setting a programmed rate of temperature rise on a surface of the body in a range of 10° C./h˜20° C./h.

4. The method for manufacturing a ceramic honeycomb structure according to claim 2 , wherein the body is heated in the first heating such that an organic ingredient in the body is substantially thermally decomposed.

5. The method for manufacturing a ceramic honeycomb structure according to claim 2 , wherein the second heating of the body includes maintaining a surface temperature of the body in a range of 450° C.˜600° C.

6. The method for manufacturing a ceramic honeycomb structure according to claim 2 , wherein the degreasing of the body includes placing the body comprising the raw material paste in a degreasing furnace and raising the oxygen concentration in the degreasing furnace to a range of 1%˜5% in 0.1˜50 hours in the second heating.

7. The method for manufacturing a ceramic honeycomb structure according to claim 2 , wherein the second heating comprises heating the body comprising the raw material paste in the atmosphere having the oxygen concentration which is higher than the oxygen concentration of the first heating such that an organic ingredient in the body is substantially oxidized.

8. The method for manufacturing a ceramic honeycomb structure according to claim 2 , further comprising drying the body comprising the raw material paste and having the honeycomb structure.

9. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the first heating of the body includes setting a programmed rate of temperature rise on a surface of the body in a range of 10° C./h˜20° C./h.

10. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the body is heated in the first heating such that an organic ingredient in the body is substantially thermally decomposed.

11. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the second heating of the body includes maintaining a surface temperature of the body in a range of 450° C.˜600° C.

12. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the degreasing of the body includes placing the body comprising the raw material paste in a degreasing furnace and raising the oxygen concentration in the degreasing furnace to a range of 1%˜5% in 0.1˜50 hours in the second heating.

13. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the second heating comprises heating the body comprising the raw material paste in the atmosphere having the oxygen concentration which is higher than the oxygen concentration of the first heating such that an organic ingredient in the body is substantially oxidized.

14. The method for manufacturing a ceramic honeycomb structure according to claim 1 , further comprising drying the body comprising the raw material paste and having the honeycomb structure.

15. The method for manufacturing a ceramic honeycomb structure according to claim 1 , further comprising applying a sealant to one end of each of the through-holes of the body in the longitudinal direction such that each of the through-holes of the body is sealed at the one end.

16. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the inorganic particles are at least one inorganic particle material selected from the group consisting of silicon carbide particles, titania particles and alumina particles.

17. The method for manufacturing a ceramic honeycomb structure according to claim 1 , further comprising forming a precursor comprising particles comprising the inorganic particles, wherein the kneading comprises kneading the binder ingredient and the particles of the precursor comprising the inorganic particles, and the inorganic particles are titania particles and alumina particles.

18. The method for manufacturing a ceramic honeycomb structure according to claim 17 , wherein the forming of the precursor comprises spray-drying the alumina particles onto the titania particles.

19. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the body is heated in the first heating such that a first organic ingredient in the body is substantially thermally decomposed, and the second heating comprises heating the body comprising the raw material paste in the atmosphere having the oxygen concentration which is higher than the oxygen concentration of the first heating such that a second organic ingredient in the body is substantially oxidized.

Assignees

• Ibiden Co Ltd

Inventors

• Yamayose Kazunori

Classifications

• B28B21/92 Primary

  Methods or apparatus for treating or reshaping · CPC title

• C04B35/478 Primary

  based on aluminium titanates · CPC title

• C04B2235/3217

  Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina · CPC title

• C04B2235/6567

  Treatment time · CPC title

• C04B35/62655

  Drying, e.g. freeze-drying, spray-drying, microwave or supercritical drying · CPC title