Compressed fiber structural material and method for producing the same

Patent metadata

Field	Value
Publication number	US-9320602-B2
Application number	US-201214345668-A
Country	US
Kind code	B2
Filing date	Mar 9, 2012
Priority date	Sep 20, 2011
Publication date	Apr 26, 2016
Grant date	Apr 26, 2016

Abstract

Provided is a method for easily producing a lamellar compressed fiber structural material which has mechanical characteristics close to those of in vivo bone and which is capable of easily increasing osteoblast even when a difference in strength exists. In order to solve the issues, the method for producing compressed fiber structural material 1 , includes: a step of preparing biocompatible fiber 14 having an average diameter of 5 μm-50 μm and an aspect ratio of 20-500; and a step of molding compressed fiber structural material 1 by cold pressing/shearing biocompatible fiber 14 , compressed fiber structural material 1 having an average pore diameter that is in the range of 60 μm-100 μm inclusive and a void fraction that is in the range of 25%-50% inclusive, both obtained by measurement in accordance with the mercury penetration method. Further, it is preferable for the cold pressing/shearing is performed by controlling a compressive pressure in the range of 200 MPa-2000 MPa, a shearing stroke length in the range of 0.2 mm-5 mm and a shearing velocity in the range of 0.5 mm/min-5 mm/min.

First claim

The invention claimed is:

1. A method for producing a compressed fiber structural material, comprising:
a step of preparing a biocompatible fiber having an average diameter of 5 μm-50 μm and an aspect ratio of 20-500; and
a step of molding a compressed fiber structural material by cold pressing/shearing the biocompatible fiber, the compressed fiber structural material having an average pore diameter that is in the range of 60 μm-100 μm inclusive and a void fraction that is in the range of 25%-50% inclusive, both obtained by measurement in accordance with the mercury penetration method, wherein
a titanium fiber is used as the biocompatible fiber, and
the step of molding a compressed fiber structural material includes:
a step of obtaining the primary compressed compact by cold pressing/shearing the biocompatible fiber; and
a step of secondary-molding the primary compressed compact that is sandwiched by the magnesium powder from the top and the bottom or that has the magnesium powder deposited on either one of the top and the bottom.

2. The method for producing a compressed fiber structural material according to claim 1 , wherein
the cold pressing/shearing is performed by controlling a compressive pressure in the range of 200 MPa-2000 MPa, a shearing stroke length in the range of 0.2 mm-5 mm and a shearing velocity in the range of 0.5 mm/min-5 mm/min.

3. The method for producing a compressed fiber structural material according to claim 1 , wherein
a bulk density of the compressed fiber structural material is controlled so as to be in the range of 3 g/cm 3 -5 g/cm 3 .

4. A compressed fiber structural material, comprising:
a biocompatible fiber having an average diameter of 5 μm-50 μm and an aspect ratio of 20-500, the biocompatible fiber being compressed and solidified without sintering, the biocompatible fiber being a titanium fiber as a compressed compact;
magnesium powders deposited on at least one of the top surface and the bottom surface of the compressed compact, the magnesium powders being compressed and solidified without sintering; and
an average pore diameter in the range of 60 μm-100 μm inclusive and a void fraction in the range of 25%-50% inclusive, both of the average pore diameter and the void fraction being obtained by measurement in accordance with the mercury penetration method.

5. The compressed fiber structural material according to claim 4 , wherein
a bulk density of the compressed fiber structural material is controlled so as to be in the range of 3 g/cm 3 -5 g/cm 3 .

Assignees

• Nakayama Noboru
• Horita Masaomi
• Izawa Naoki
• Tamai Hiroto
• Saito Naoto
• Usui Yuki
• Ogihara Nobuhide
• Univ Shinshu

Inventors

• Nakayama Noboru
• Horita Masaomi
• Izawa Naoki
• Tamai Hiroto
• Saito Naoto
• Usui Yuki
• Ogihara Nobuhide

Classifications

• A61L27/04 Primary

  Metals or alloys · CPC title

• C22F1/183

  of titanium or alloys based thereon · CPC title

• C22C49/11

  Titanium · CPC title

• A61F2/28 Primary

  Bones · CPC title

• A61F2310/00023

  Titanium or titanium-based alloys, e.g. Ti-Ni alloys · CPC title