Device for producing ethanol and method for producing ethanol

Patent metadata

Field	Value
Publication number	US-9308469-B2
Application number	US-201113809269-A
Country	US
Kind code	B2
Filing date	Jul 21, 2011
Priority date	Jul 22, 2010
Publication date	Apr 12, 2016
Grant date	Apr 12, 2016

Abstract

Disclosed are a method for producing ethanol and a device for producing ethanol that are suitable to the recycled use of an enzyme.
The device is configured from: a vacuum distillation tower ( 11 ) into which an ethanol-fermented liquid generated by saccharification fermentation of a biomass starting material is introduced, and with the interior in a state that is at a lower pressure than atmospheric pressure, that subjects the ethanol-fermented liquid to distillation, distilling ethanol vapor that contains water vapor, and removing as a bottom product the enzyme-containing concentrated waste liquid that is roused for saccharification fermentation of the biomass starting material; and a fractionating tower ( 12 ) for fractionating the ethanol vapor distilled from the vacuum distillation tower ( 11 ). In this case, the energy of the ethanol vapor can be more efficiently taken advantage of if the device is provided with a first compressor ( 16 ) that adiabatically compresses the ethanol vapor distilled from the vacuum distillation tower ( 11 ), and the ethanol vapor adiabatically compressed by the first compressor ( 16 ) is introduced into the fractionating tower ( 12 ).

First claim

The invention claimed is:

1. A method for producing ethanol by purifying ethanol from an ethanol-fermented liquid containing a diastatic enzyme and 1 to 10% ethanol generated by saccharification fermentation of a pretreated biomass starting material, the method comprising:
a step of pretreating a biomass starting material to enhance enzyme reactivity to form a pretreated biomass starting material comprising pulp;
a step of subjecting the pretreated biomass starting material to saccharification fermentation to form the ethanol-fermented liquid;
a step of subjecting the ethanol-fermented liquid containing the diastatic enzyme and 1 to 10% ethanol to vacuum distillation to produce an ethanol vapor containing water vapor and an enzyme-containing concentrated waste liquid;
a step of adiabatically compressing the ethanol vapor to increase the temperature and the pressure of the ethanol vapor;
a step of rectifying the ethanol vapor; and
a step of recycling the enzyme-containing concentrated waste liquid to a step of subjecting the pretreated biomass starting material to saccharification fermentation,
wherein the method further comprises a step of adjusting a flow rate of the ethanol vapor from the step of subjecting the ethanol-fermented liquid to vacuum distillation to produce ethanol vapor containing water vapor and the enzyme-containing concentrated waste liquid so that a weight of the enzyme-containing concentrated waste liquid from the step of subjecting the ethanol-fermented liquid to vacuum distillation to produce ethanol vapor containing water vapor and the enzyme-containing concentrated waste liquid becomes 2 to 20 times as much as a pulp weight generated in the pretreatment for enhancing an enzyme reactivity of the biomass starting material.

2. The method for producing ethanol according to claim 1 , further comprising a step of heat-exchanging the ethanol vapor having been subjected to temperature increase and pressure increase by the step of adiabatically compressing the ethanol vapor with a tower bottom recycled liquid of a vacuum distillation tower to achieve condensation thereof, and wherein
the ethanol vapor from the vacuum distillation tower is introduced into the rectifying step after the ethanol vapor is converted into an ethanol liquid.

3. The method for producing ethanol according to claim 1 , wherein a part of the ethanol vapor adiabatically compressed by a first compressor used in the step of adiabatically compressing the ethanol vapor is recycled to an entry side of the first compressor.

Assignees

• Kiuchi Takafumi
• Hidaka Ryohta
• Ishibashi Yoichi
• Sumi Tomonori
• Katoh Yasuhiko
• Kansha Yasuki
• Tsutsumi Atsushi
• Nippon Steel & Sumikin Eng Co
• Univ Tokyo

Inventors

• Kiuchi Takafumi
• Hidaka Ryohta
• Ishibashi Yoichi
• Sumi Tomonori
• Katoh Yasuhiko
• Kansha Yasuki
• Tsutsumi Atsushi

Classifications

• C12M21/12 Primary

  for producing fuels or solvents (C12M21/04 takes precedence; liquid carbonaceous fuels C10L1/00, solid fuels C10L5/00) · CPC title

• C12M47/10

  Separation or concentration of fermentation products (bioreactors combined with means for distillation or extraction of liquid fuel C12M43/02) · CPC title

• Y02E50/16

  Cross-Sectional Technologies · mapped topic

• C12P7/06

  Ethanol, i.e. non-beverage · CPC title

• B01D3/143 Primary

  by two or more of a fractionation, separation or rectification step · CPC title