Apparatus for conducting simulated countercurrent adsorptive separation of a multi-component feed stream

Patent metadata

Field	Value
Publication number	US-9302201-B2
Application number	US-201314036028-A
Country	US
Kind code	B2
Filing date	Sep 25, 2013
Priority date	Mar 30, 2010
Publication date	Apr 5, 2016
Grant date	Apr 5, 2016

Abstract

A process for separating a product from a multicomponent feedstream to an adsorption apparatus or system is described. The apparatus or system may comprise a moving-bed or a simulated moving-bed adsorption means. The product comprises at least one organic compound, such as an aryl compound with alkyl substitutes. In embodiments the conduits used to supply the feedstream to the apparatus or system are flushed with media of multiple grades. The improvement is more efficient use of the desorbent. In embodiments the process achieves improvements in one or more of efficiency of adsorption separation, capacity of adsorption apparatus systems, and purity of product attainable by adsorption process.

First claim

What is claimed is:

1. An apparatus adapted for a process for separating a product from at least one multicomponent feed by simulated countercurrent adsorptive separation comprising plural sieve chambers fluidly connected with plural bedlines A 1 through A n+j , wherein n>2 and n+j is the total number of bedlines, which in turn are fluidly connected with a matrix of fluid communication conduits to distribute plural input streams, including desorbent, a primary flush, a secondary flush, and at least one multicomponent feed, and plural output streams, including a primary flush output and a secondary flush output, extract comprising the product, and raffinate, from said plural sieve chambers, the improvement characterized by a fluid connection between the primary flush output communication conduit and the secondary flush input communication conduit, whereby the primary flush output may be routed directly for use as the secondary flush without being routed through intervening distillation apparatus, and wherein the secondary flush input enters a bedline (A n+4 ) four bedlines upstream of the bedline (A n ) from which the extract is withdrawn.

Assignees

• Exxonmobil Chem Patents Inc

Inventors

• Porter John R
• Pilliod Dana L

Classifications

• C07C7/13

  by molecular-sieve technique · CPC title

• B01D15/1835 Primary

  Flushing · CPC title

• Y02P20/52

  using catalysts, e.g. selective catalysts · CPC title

• B01J21/00

  Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium · CPC title

• B01D53/08 Primary

  according to the "moving bed" method · CPC title