Magnetic material and coil component using the same

Patent metadata

Field	Value
Publication number	US-9293244-B2
Application number	US-201213546911-A
Country	US
Kind code	B2
Filing date	Jul 11, 2012
Priority date	Jul 19, 2011
Publication date	Mar 22, 2016
Grant date	Mar 22, 2016

Abstract

A magnetic material constituted by a grain compact 1 obtained by shaping metal grains 11 and then heat-treating them in an oxidizing ambience, wherein the metal grains 11 are made of a Fe—Cr—Si alloy and their Fe Metal /(Fe Metal +Fe Oxide ) ratio as measured before shaping by XPS, with respect to the sum of integral values at the peaks of 709.6 eV, 710.7 eV and 710.9 eV, or Fe Oxide , and peak integral value at 706.9 eV, or Fe Metal , is 0.2 or more.

First claim

We claim:

1. A method of manufacturing a magnetic material, comprising:
selecting metal grains which are made of a Fe—Cr—Si alloy and whose Fe Metal /(Fe Metal +Fe Oxide ) ratio as measured before shaping by XPS is 0.2 or more wherein Fe Oxide is the sum of integral values at peaks of 709.6 eV, 710.7 eV and 710.9 eV, and Fe Metal is a peak integral value at 706.9 eV; and
shaping a formed body using the metal grains; and
heating the formed body to obtain a grain compact as a magnetic material,
wherein the step of selecting the metal grains comprises providing metal grains; measuring the Fe Metal /(Fe Metal +Fe Oxide ) ratio; if the ratio is not 0.2 or more, treating the metal grains with acid or with heat in a reducing ambience.

2. The method according to claim 1 , wherein the step of shaping the formed body is conducted under a non-heated condition.

3. The method according to claim 1 , wherein the step of shaping the formed body comprises mixing the metal grains with an organic resin as a binder.

4. The method according to claim 1 , wherein the step of heating the formed body is conducted in an oxidizing ambience.

5. The method according to claim 1 , wherein the step of heating the formed body is conducted under conditions such that the formation of both oxide film bond between the metal grains and metal bond between the metal grains is facilitated.

6. The method according to claim 1 , wherein the Cr content in the grain compact is 2.0 to 15 percent by weight.

7. The method according to claim 1 , wherein the grain size distribution of metal grains before shaping, based on volume, is such that d10/d50 is 0.1 to 0.7 and d90/d50 is 1.4 to 5.0.

8. The method according to claim 1 , wherein the tap density of metal grains before shaping, as specified in the Japanese Industrial Standard (JIS) Z 2512:2006, is 3.8 g/cm 3 or more.

Assignees

• Matsuura Hitoshi
• Ogawa Hideki
• Tanada Atsushi
• Tanaka Kiyoshi
• Otake Kenji
• Taiyo Yuden Kk

Inventors

• Matsuura Hitoshi
• Ogawa Hideki
• Tanada Atsushi
• Tanaka Kiyoshi
• Otake Kenji

Classifications

• H01F1/33

  mixtures of metallic and non-metallic particles; metallic particles having oxide skin · CPC title

• H01F1/14766

  Fe-Si based alloys · CPC title

• H01F1/01

  of inorganic materials (H01F1/44 takes precedence) · CPC title

• H01F41/0246

  Manufacturing of magnetic circuits by moulding or by pressing powder (magnetic cores made by moulding or by pressing powder H01F27/255; soft magnetic particles H01F1/20, H01F1/36) · CPC title

• H01F27/255 Primary

  made from particles (H01F27/26 takes precedence) · CPC title