Activated charcoal

Patent metadata

Field	Value
Publication number	US-9290390-B2
Application number	US-201113521445-A
Country	US
Kind code	B2
Filing date	Jan 10, 2011
Priority date	Jan 11, 2010
Publication date	Mar 22, 2016
Grant date	Mar 22, 2016

Abstract

The invention provides a method for preparing activated charcoal from a precursor material comprising high mineral content plant or algal material by heating the precursor material under suitable conditions sufficient to produce activated charcoal therefrom. The invention also provides various applications of the activated charcoal per se.

First claim

What is claimed is:

1. A method of making activated charcoal, comprising:
heating a precursor material having a high mineral content to a temperature of between 600° C.-1000° C., for at least 10 minutes to obtain an activated charcoal, wherein the concentration of alkali and/or alkaline earth metals of the precursor material in a dry state is at least 20,000 mg/kg; and no exogenous activating material is added to obtain the activated charcoal and washing the activated charcoal with acid to remove an activating mineral ion to reveal a pore structure; and collecting the mineral ion in the acid wash.

2. The method of claim 1 , wherein the alkali and/or alkaline earth metals comprise is at least one of a magnesium, sodium, calcium and potassium.

3. The method of claim 1 , wherein the pore structure of the activated carbon comprises at least one of meso pore and micro pore; wherein the meso- and micro-pore volumes are at least one of a 0.2 cm 3 g −1 , 0.5 cm 3 g −1 , and 0.8 cm 3 g −1 , and wherein the activated charcoal comprises mesoporosity of at least 30%.

4. The method of claim 1 , further comprising:
separating the resultant activated carbon from the dissolved minerals.

5. A method according to claim 1 , wherein the concentration of alkali and/or alkaline earth metals is at least 60,000 mg/kg of the precursor material in a dry state.

6. A method according to claim 2 , wherein the concentration of potassium is at least 10,000 mg/kg of the precursor material in a dry state, and/or the concentration of magnesium is at least 1,000 mg/kg of the precursor material in a dry state, and/or the concentration of calcium is at least 3,000 mg/kg of the precursor material in a dry state, and/or the concentration of sodium is at least 1,000 mg/kg of the precursor material in a dry state.

7. A method according to claim 1 , wherein the precursor material comprises of a hardwood species of plant or a softwood species of plant.

8. A method according to claim 1 , wherein the precursor material is a non-woody plant material selected from the group consisting of Brassicaceae, Amaranthaceae, Urticaceae, Spinacea oleracea (spinach), Brassica napus (oilseed rape) and Beta vulgaris (sea beet, mangel-wurzel, and swiss chard).

9. A method according to claim 1 , wherein the precursor material comprises algae and the algae comprises of macroalgae or microalgae, wherein the precursor material comprises of seaweed, such as channel wrack, flat wrack, knotted wrack, bladder wrack, saw wrack, thong weed, kelp, oar weed and sea lettuce.

10. A method according to claim 9 , wherein the algae is derived from the family Fucaceae or Euglenaceae.

11. A method according to claim 1 , wherein the precursor material is heated to a temperature of at least 700° C.

12. A method according to claim 4 , wherein, following separation from the acid, the method comprises adjusting the pH of the resultant activated carbon until the pH indicates that the majority of the acid has been neutralized, optionally wherein pH adjustment is achieved by washing with water.

Assignees

• De Leij Franciscus Antonius Anna Maria
• Stratford James Peter
• Univ Surrey

Inventors

• De Leij Franciscus Antonius Anna Maria
• Stratford James Peter

Classifications

• C01B32/318

  characterised by the starting materials · CPC title

• C05G3/80

  Soil conditioners · CPC title

• C01B32/30 Primary

  Active carbon · CPC title

• C01B32/324

  from waste materials, e.g. tyres or spent sulfite pulp liquor · CPC title

• B01J20/28088

  Pore-size distribution · CPC title