Methods for reducing impurities in magnesium, purified magnesium, and zirconium metal production methods
US-10422017-B2 · Sep 24, 2019 · US
US9284622B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9284622-B2 |
| Application number | US-201214006303-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 16, 2012 |
| Priority date | Mar 23, 2011 |
| Publication date | Mar 15, 2016 |
| Grant date | Mar 15, 2016 |
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A device and a method for removing impurities in an aluminum melt are provided, in which the device includes an upper furnace body, a lower furnace body, an intermediate partition plate, a crucible, heating elements and a charging opening. The intermediate partition plate is mounted between the upper furnace body and the lower furnace body. The upper furnace body, a mixing chamber and a heating element are above the intermediate partition plate. The crucible is mounted in the lower furnace body. A heating element is provided around the lower furnace body. The mixing chamber and the crucible are connected by a jet pipe passing through the intermediate partition plate. For the device and the method, impurity removal is quick, efficiency is high and the process is closed, so there is no environmental pollution, and the aluminum melt after impurity removal may be directly cast.
Opening claim text (preview).
The invention claimed is: 1. A device for removing impurities in aluminum melt comprising: an upper furnace body, a lower furnace body, an intermediate partition plate, a crucible, heating elements, and a charging opening, wherein: the intermediate partition plate is mounted between the upper furnace body and the lower furnace body; the upper furnace body, a mixing chamber and a heating element are provided above the intermediate partition plate; the crucible is mounted inside the lower furnace body; a heating element is provided in the lower furnace body; the lower furnace body is provided with the charging opening and a pipeline; the upper furnace body is provided with an inlet valve and an exhaust valve; the mixing chamber and the crucible are connected via a jet pipe passing through the intermediate partition plate; and a ceramic seal pad is provided between the mixing chamber and the jet pipe for sealing. 2. The device for removing impurities in aluminum melt according to claim 1 , wherein the mixing chamber is a cylinder or a polygonal canister, wherein the bottom of the mixing chamber is cambered or flat and comprises an opening. 3. A method for removing impurities in aluminum melt with the device according to claim 1 , comprising the following steps: placing a furnace burden and a flux in the crucible, heating the lower furnace body with the heating element, so that the furnace burden and the flux are melted and liquid flux covers aluminum melt; mounting the intermediate partition plate, the jet pipe, the ceramic seal pad, the mixing chamber and the upper furnace body when the temperature of the aluminum melt is up to 700° C.-720° C., clamping and sealing the upper furnace body, the lower furnace body and the intermediate partition plate are clamped and sealed with a quick opening fixture, heating the upper furnace body with the heating element so that the temperature of the mixing chamber reaches 700° C.; opening the inlet valve and the exhaust valve, wherein an inert gas is charged via the inlet valve into the upper furnace body so as to expel air in the upper furnace body via the exhaust valve, in order to prevent the aluminum melt entering into the mixing chamber from being oxidized when contacting with the air; opening an adjustable valve to charge dry compressed air or inert gas from a gas source into the lower furnace body, so that the pressure of the lower furnace body is increased gradually; wherein, under the increase of the pressure, the aluminum melt in the crucible stably flows into the mixing chamber along the jet pipe, then the liquid flux enters into the mixing chamber via the jet pipe in a manner of confined jet flow and uniformly mixes with the aluminum melt, so that the impurities in the aluminum melt are transferred to the liquid flux; closing the adjustable valve when a level of the liquid flux in the crucible descends near to the inlet of the jet pipe; and opening another adjustable valve so that the lower furnace body is communicated with a surrounding atmosphere; wherein the mixture of aluminum melt and the liquid flux in the mixing chamber flows back into the crucible along the jet pipe under gravity, and the liquid flux re-floats on the aluminum melt, whereby a working cycle is completed, and the above-mentioned steps are repeated for several times until a satisfactory impurity removing effect is achieved. 4. The method for removing impurities in aluminum melt according to claim 3 , wherein the furnace burden comprises aluminum alloys and aluminum matrix composites. 5. The method for removing impurities in aluminum melt according to claim 3 , wherein the flux comprises a mixture of three or four ingredients selected from the group consisting of NaCl, KCl, NaF and Na 3 AlF 6 , wherein the melting point of the mixture is not more than 700° C. 6. A method for removing impurities in aluminum melt with the device according to claim 1 , comprising the following steps: mounting the intermediate partition plate, the jet pipe, the ceramic seal pad and the mixing chamber, mounting the upper furnace body, clamping and sealing the upper furnace body, the lower furnace body and the intermediate partition plate with a quick opening fixture, heating the lower furnace body with the heating element in the lower furnace body; opening the charging opening, pouring an aluminum melt and a liquid flux, both of which have been melted by another furnace into the crucible via the charging opening of the lower furnace body; heating the upper furnace body with the heating element when the temperature of the aluminum melt is up to 700° C.-720° C. so that the temperature of the mixing chamber reaches 700° C.; opening the inlet valve and the exhaust valve, wherein an inert gas is charged via the inlet valve into the upper furnace body so as to expel air in the upper furnace body via the exhaust valve, in order to prevent the aluminum melt entering into the mixing chamber from being oxidized when contacting with the air; opening an adjustable valve to charge dry compressed air or an inert gas from a gas source into the lower furnace body, so that the pressure of the lower furnace body is increased gradually; wherein, under the increase of the pressure, the aluminum melt in the crucible stably flows into the mixing chamber along the jet pipe, then the liquid flux enters into the mixing chamber via the jet pipe in a manner of confined jet flow and uniformly mixes with the aluminum melt, so that the impurities in the aluminum melt are transferred to the liquid flux; closing the adjustable valve when a level of the liquid flux in the crucible descends near to the inlet of the jet pipe, and opening another adjustable valve so that the lower furnace body is communicated with a surrounding atmosphere; wherein the mixture of aluminum melt and the liquid flux in the mixing chamber flows back into the crucible along the jet pipe under gravity, and the liquid flux re-floats on the aluminum melt, whereby a working cycle is completed, and the above-mentioned steps are repeated for several times until a satisfactory impurity removing effect is achieved.
Pots, e.g. slag pots, ladles · CPC title
Stirring devices for molten material (charging or discharging liquid or molten material F27D3/14) · CPC title
with refining or fluxing agents; Use of materials therefor, {e.g. slagging or scorifying agents}(C22B9/18 takes precedence){(C22B9/006 takes precedence)} · CPC title
using salt or fluxing agents (C22B21/064, C22B21/066, and C22B21/068 take precedence) · CPC title
combined in one structure · CPC title
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