Heat integrated distillation apparatus

Patent metadata

Field	Value
Publication number	US-9278295-B2
Application number	US-201313771741-A
Country	US
Kind code	B2
Filing date	Feb 20, 2013
Priority date	Feb 20, 2012
Publication date	Mar 8, 2016
Grant date	Mar 8, 2016

Abstract

A distillation apparatus includes a rectifying column, a stripping column, a first pipe that communicates a column top of the stripping column with a column bottom of the rectifying column, and a compressor configured to compress vapor from the stripping column and then to feed the compressed vapor to the rectifying column. The distillation apparatus further includes a heat exchanger located at a predetermined stage of the rectifying column, a liquid withdrawal unit located at a predetermined stage of the stripping column and configured to withdraw a part of liquid from the predetermined stage to an outside of the column, a second pipe that introduces the liquid from the liquid withdrawal unit to the heat exchanger, and a third pipe that introduces fluids introduced through the second pipe to the heat exchanger and then discharged out of the heat exchanger to a stage directly below the liquid withdrawal unit.

First claim

What is claimed is:

1. A heat integrated distillation apparatus comprising:
a rectifying column including a trayed section or a packed bed section, which is used as a rectifying section;
a stripping column located higher than said rectifying column and including a trayed section or a packed bed section, which is used as a stripping section;
a first pipe that connects a top space of said stripping column with a bottom space of said rectifying column;
a compressor installed in said first pipe and configured to compress vapor from the top space of said stripping column and then feeding the compressed vapor to the bottom space of said rectifying column;
a heat exchanger located at the trayed section or the packed bed section of said rectifying column;
a liquid withdrawal unit located at the trayed section or the packed bed section of said stripping column and configured to remove a part of liquid from the trayed section or the packed bed section of said stripping column to an outside of the column;
a second pipe that introduces the liquid from said liquid withdrawal unit to said heat exchanger; and
a third pipe that introduces fluids introduced through said second pipe to said heat exchanger and then discharged from the heat exchanger, to a stage directly below said liquid withdrawal unit of the stripping section,
wherein a bottom space of said stripping column and a top space of said rectifying column are located in positions at a same column elevation.

2. The heat integrated distillation apparatus according to claim 1 ,
wherein said rectifying column and said stripping column are formed by a partition wall that divides an inside of one column into two, and the partition wall partitions the inside of the column so that the bottom space of said stripping column and the top space of said rectifying column are located in the positions at the same column elevation.

3. The heat integrated distillation apparatus according to claim 1 , further comprising a raw material supply pipe that supplies a raw material to at least one of the top space of said stripping column and one of the trayed section of said stripping column and the packed bed section of said stripping column.

4. The heat integrated distillation apparatus according to claim 3 , further comprising a pump and a pipe that pressure-feeds liquid in the bottom space of said rectifying column to said raw material supply pipe.

5. The heat integrated distillation apparatus according to claim 1 , further comprising a reboiler that heats liquid in the bottom space, outside the bottom space of said stripping column.

6. The heat integrated distillation apparatus according to claim 1 , further comprising a condenser that cools vapor in the top space, outside the top space of said rectifying column.

Assignees

• Toyo Engineering Corp

Inventors

• Wakabayashi Toshihiro
• Nakao Takato

Classifications

• B01D3/007 Primary

  Energy recuperation; Heat pumps · CPC title

• B01D3/143

  by two or more of a fractionation, separation or rectification step · CPC title

• B01D1/28 Primary

  with vapour compression · CPC title

• B01D3/141

  where at least one distillation column contains at least one dividing wall · CPC title

• B01D3/00

  Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping ({evaporation in general, e.g. of liquids for gas phase reactions B01B1/005;} gas chromatography B01D15/08; destructive distillation C10B; preparation of alcoholic beverages by distillation C12H6/02) · CPC title