Sputtering target of magnetic material

Patent metadata

Field	Value
Publication number	US-9269389-B2
Application number	US-201013513387-A
Country	US
Kind code	B2
Filing date	Oct 21, 2010
Priority date	Dec 11, 2009
Publication date	Feb 23, 2016
Grant date	Feb 23, 2016

Abstract

A magnetic sputtering target which contains B and is obtained by a melting and casting method, wherein the B content is 10 at % or more and 50 at % or less, and the remainder is one or more elements selected from Co, Fe, and Ni. Based on the method of the present invention, the sputtering target, in which gaseous impurities are few, there are no cracks and fractures, and segregation of its main constituent elements is minimal, is obtained. Consequently, when sputtered with a magnetron sputtering device comprising a DC power supply, this sputtering target yields a significant effect of being able to inhibit the generation of particles during sputtering, and improve the production yield upon forming thin films.

First claim

The invention claimed is:

1. A sputtering target of a magnetic material, having a cast structure obtained by melting and succeeding casting, wherein the sputtering target has a composition consisting of B in an amount of 10 at % or more and 50 at % or less, one or more elements selected from the group consisting of Co, Fe, and Ni, and impurity oxygen in an amount of 100 wtppm or less, and wherein the sputtering target has a location to location variation of B content defined as (Am−A)/A in an amount of 0.01 or less within the sputtering target, where A is a content of B of the sputtering target as a whole and Am is a content of B analyzed for an arbitrarily selected location having an area of 1 mm square within the target.

2. A sputtering target of a magnetic material, having a cast structure obtained by melting and succeeding casting, wherein the sputtering target has a composition consisting of B in an amount of 10 at % or more and 50 at % or less, one or more elements selected from the group consisting of Al, Cu, Mn, Nb, Ta, and Zr in an amount of 0.5 at % or more and 10 at % or less, one or more elements selected from the group consisting of Co, Fe, and Ni, and impurity oxygen in an amount of 100 wtppm or less, and wherein the sputtering target has a location to location variation of B content defined as (Am−A)/A in an amount of 0.01 or less within the sputtering target, where A is a content of B of the sputtering target as a whole and Am is a content of B analyzed for an arbitrarily selected location having an area of 1 mm square within the target.

3. A method of producing a sputtering target of a magnetic material having a cast structure, comprising the steps of: preparing an ingot by melting and casting a raw material having a composition consisting of B in an amount of 10 at % or more and 50 at % or less, one or more elements selected from the group consisting of Co, Fe, and Ni, and impurity oxygen in an amount of 100 wtppm or less; and cutting and machining the ingot to obtain a target, wherein the sputtering target has a location to location variation of B content defined as (Am−A)/A in an amount of 0.01 or less within the sputtering target, where A is a content of B of the sputtering target as a whole and Am is a content of B analyzed for an arbitrarily selected location having an area of 1 mm square within the target.

4. The method of producing a sputtering target of magnetic material according to claim 3 , wherein the ingot is prepared by performing rapid cooling at a rate of 30 to 60° C./minute after the melting process.

5. The method of producing a sputtering target of magnetic material according to claim 4 , wherein the rapidly cooled ingot is further subject to heat treatment in a range of 800 to 1100° C. when the B content is 30 at % or less, or in a range of 850 to 1150° C. when the B content exceeds 30 at %.

6. The method of producing a sputtering target of magnetic material according to claim 5 , wherein the target is obtained by cutting and machining the ingot after the heat treatment.

7. A method of producing a sputtering target of a magnetic material having a cast structure, comprising the steps of: preparing an ingot by melting and casting a raw material having a composition consisting of B in an amount of 10 at % or more and 50 at % or less, one or more elements selected from Al, Cu, Mn, Nb, Ta, and Zr in an amount of 0.5 at % or more and 10 at % or less, one or more elements selected from the group consisting of Co, Fe, and Ni, and impurity oxygen in an amount of 100 wtppm or less; and cutting and machining the ingot to obtain a target, wherein the sputtering target has a location to location variation of B content defined as (Am−A)/A in an amount of 0.01 or less within the sputtering target, where A is a content of B of the sputtering target as a whole and Am is a content of B analyzed for an arbitrarily selected location having an area of 1 mm square within the target.

8. The method of producing a sputtering target of magnetic material according to claim 7 , wherein the ingot is prepared by performing rapid cooling at a rate of 30 to 60° C./minute after the melting process.

9. The method of producing a sputtering target of magnetic material according to claim 8 , wherein the rapidly cooled ingot is further subject to heat treatment in a range of 800 to 1100° C. when the B content is 30 at % or less, or in a range of 850 to 1150° C. when the B content exceeds 30 at %.

10. The method of producing a sputtering target of magnetic material according to claim 9 , wherein the target is obtained by cutting and machining the ingot after the heat treatment.

Assignees

• Arakawa Atsutoshi
• Jx Nippon Mining & Metals Corp

Inventors

• Arakawa Atsutoshi

Classifications

• C22C38/002

  containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60 · CPC title

• G11B5/851 Primary

  Coating a support with a magnetic layer by sputtering · CPC title

• C22C19/07

  based on cobalt · CPC title

• C22C38/10

  containing cobalt · CPC title

• C22C38/105

  containing Co and Ni · CPC title