Process for preparing phosphorus containing cyanohydrins
US-9850263-B2 · Dec 26, 2017 · US
US9255115B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9255115-B2 |
| Application number | US-201214348376-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 28, 2012 |
| Priority date | Sep 30, 2011 |
| Publication date | Feb 9, 2016 |
| Grant date | Feb 9, 2016 |
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The present invention provides a method for producing crystalline glufosinate P free acid with high purity from glufosinate P hydrochloride salt. In addition, the present invention also provides a method comprises a process of: dissolving glufosinate P hydrochloride salt in a solvent which is a mixed solvent of water and an alcohol(s) selected from the group of methanol, ethanol, propyl alcohol and isopropyl alcohol, and a ratio of water to the alcohol(s) is from 1:3 to 1:100 by volume; crystallizing glufosinate P free acid after neutralizing by addition of a base.
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What is claimed is: 1. A method for producing a compound expressed by the following formula (I): the method comprising: dissolving a compound expressed by the following formula (II): in a solvent which is a mixed solvent of water and methanol, and a ratio…
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
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