Method of making a nanomatrix powder metal compact
US-9079246-B2 · Jul 14, 2015 · US
US9243475B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9243475-B2 |
| Application number | US-201113194361-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 29, 2011 |
| Priority date | Dec 8, 2009 |
| Publication date | Jan 26, 2016 |
| Grant date | Jan 26, 2016 |
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A powder metal compact is disclosed. The powder compact includes a substantially elongated cellular nanomatrix comprising a nanomatrix material. The powder compact also includes a plurality of substantially elongated dispersed particles comprising a particle core material that comprises Mg, Al, Zn or Mn, or a combination thereof, dispersed in the cellular nanomatrix. The powder compact further includes a bond layer extending throughout the cellular nanomatrix between the dispersed particles, wherein the cellular nanomatrix and the dispersed particles are substantially elongated in a predetermined direction.
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The invention claimed is: 1. A powder metal compact, comprising: a substantially elongated cellular nanomatrix comprising a nanomatrix material; a plurality of substantially elongated dispersed particles comprising a particle core material that comprises Mg, Al, Zn or Mn, or a combination thereof, dispersed in the cellular nanomatrix; and a solid-state bond layer formed by solid state bonding extending throughout the cellular nanomatrix between adjacent dispersed particles, wherein the cellular nanomatrix and the dispersed particles are substantially elongated in one predetermined direction to an extent that the cellular nanomatrix, dispersed particles, and solid-state bond layer are substantially continuous in the predetermined direction or to an extent that the nanomatrix and dispersed particles become separated, cracked or otherwise substantially discontinuous in the predetermined direction. 2. The powder metal compact of claim 1 , wherein the substantially elongated nanomatrix and dispersed particles exhibit a predetermined reduction ratio. 3. The powder metal compact of claim 2 , wherein the predetermined reduction ratio is from about 5 to about 2000. 4. The powder metal compact of claim 3 , wherein the predetermined reduction ratio is from about 50 to about 1000. 5. The powder metal compact of claim 1 , wherein the particle core material comprises Mg-Zn, Mg-Zn, Mg-Al, Mg-Mn, Mg-Zn-Y or an Mg-Al-X alloy, wherein X comprises Zn, Mn, Si, Ca or Y, or a combination thereof. 6. The powder metal compact of claim 1 , wherein the dispersed particles further comprise a rare earth element. 7. The powder metal compact of claim 1 , wherein the powder compact is formed from a precursor compact having dispersed particles have an average particle size of about 50 nm to about 500μm. 8. The powder metal compact of claim 1 , wherein the dispersion of dispersed particles comprises a substantially homogeneous dispersion within the cellular nanomatrix. 9. The powder metal compact of claim 1 , wherein the dispersion of dispersed particles comprises a multi-modal distribution of particle sizes within the cellular nanomatrix. 10. The powder metal compact of claim 1 , further comprising a plurality of substantially elongated dispersed second particles, wherein the dispersed second particles are also dispersed within the cellular nanomatrix and with respect to the dispersed particles, and wherein the dispersed second particles comprise Fe, Ni, Co or Cu, or oxides, nitrides, carbides, intermetallics or cermets thereof, or a combination of any of the aforementioned materials. 11. The powder metal compact of claim 1 , wherein the nanomatrix material comprises Al, Zn, Mn, Mg, Mo, W, Cu, Fe, Si, Ca, Co, Ta, Re or Ni, or an oxide, carbide, nitride, intermetallic or cermet thereof, or a combination of any of the aforementioned materials, and wherein the nanomatrix material has a chemical composition and the particle core material has a chemical composition that is different than the chemical composition of the nanomatrix material. 12. The powder metal compact of claim 1 , wherein the particle core material comprises pure Mg and has an ultimate compressive strength of at least about 50 ksi. 13. The powder metal compact of claim 1 , wherein the compact is formed from a sintered powder comprising a plurality of powder particles, each powder particle having a particle core that upon sintering comprises a dispersed particle and a single metallic coating layer disposed thereon, and wherein the cellular nanomatrix between adjacent ones of the plurality of dispersed particles comprises the single metallic coating layer of one powder particle, the bond layer and the single metallic coating layer of another of the powder particles. 14. The powder metal compact of claim 13 , wherein the dispersed particles comprise Mg and the cellular nanomatrix comprises Al or Ni, or a combination thereof. 15. A powder metal compact, comprising a substantially elongated cellular nanomatrix comprising a nanomatrix material; a plurality of substantially elongated dispersed particles comprising a particle core material that comprises Mg, Al, Zn or Mn, or a combination thereof, dispersed in the cellular nanomatrix; and a bond layer extending throughout the cellular nanomatrix between the dispersed particles, wherein the cellular nanomatrix and the dispersed particles are substantially elongated in one predetermined direction, and wherein the nanomatrix and the dispersed particles are elongated in the predetermined direction to an extent that the nanomatrix and dispersed particles become separated, cracked or otherwise substantially discontinuous in the predetermined direction. 16. The powder metal compact of claim 15 , wherein the substantially discontinuous nanomatrix and dispersed particles comprise substantially discontinuous strings of nanomatrix material and particle core material, respectively, oriented in the predetermined direction. 17. A powder metal compact, comprising: a substantially elongated cellular nanomatrix comprising a nanomatrix material; a plurality of substantially elongated dispersed particles comprising a particle core material that comprises Mg, Al, Zn or Mn, or a combination thereof, dispersed in the cellular nanomatrix; and a bond layer extending throughout the cellular nanomatrix between the dispersed particles, wherein the cellular nanomatrix and the dispersed particles are substantially elongated in one predetermined direction, and wherein the compact is formed from a sintered powder comprising a plurality of powder particles, each powder particle having a particle core that upon sintering comprises a dispersed particle and a plurality of metallic coating layers disposed thereon, and wherein the cellular nanomatrix between adjacent ones of the plurality of dispersed particles comprises the plurality of metallic coating layers of one powder particle, the bond layer and plurality of metallic coating layers of another of the powder particles, and wherein adjacent ones of the plurality of metallic coating layers have different chemical compositions. 18. The powder metal compact of claim 17 , wherein the plurality of layers comprises a first layer that is disposed on the particle core and a second layer that is disposed on the first layer. 19. The powder metal compact of claim 18 , wherein the dispersed particles comprise Mg and the first layer comprises Al or Ni, or a combination thereof, and the second layer comprises Al, Zn, Mn, Mg, Mo, W, Cu, Fe, Si, Ca, Co, Ta, Re or Ni, or a combination thereof, wherein the first layer has a chemical composition that is different than a chemical composition of the second layer. 20. The powder metal compact of claim 19 , metal powder of claim 18 , further comprising a third layer that is disposed on the second layer. 21. The powder metal compact of claim 20 , wherein the first layer comprises Al or Ni, or a combination thereof, the second layer comprises Al, Zn, Mn, Mg, Mo, W, Cu, Fe, Si, Ca, Co, Ta, Re or Ni, or an oxide, nitride, carbide, intermetallic or cermet thereof, or a combination of any of the aforementioned second layer materials, and the third layer comprises Al, Zn, Mn, Mg, Mo, W, Cu, Fe, Si, Ca, Co, Ta, Re or Ni, or a combination thereof, wherein the second layer has a chemical composition that is different than a chemical composition of the third layer. 22. The powder metal compact of claim 21 , further comprising a fourth layer that is disposed on the third lay
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