Apparatus and method for measuring the quantity and optical parameters of a liquid in a container using the principle of optical low coherence reflectometry

Patent metadata

Field	Value
Publication number	US-9239226-B2
Application number	US-201414162390-A
Country	US
Kind code	B2
Filing date	Jan 23, 2014
Priority date	Jan 23, 2013
Publication date	Jan 19, 2016
Grant date	Jan 19, 2016

Abstract

An apparatus for measuring the quantity and optical parameters of a liquid in a container using the principle of optical low coherence reflectometry is provided, the apparatus having: a source arm with a low coherence light source; a reference arm including a reference lens, a mirror, means for adjusting the distance between the reference lens and the mirror and means for measuring the distance between the reference lens and the mirror; a test arm with a test lens; means for dividing the output of the source arm between the test arm and the reference arm; means for combining light reflected back into the reference arm and the test arm to create an interference signal; and means for detecting and analyzing the interference signal.

First claim

What is claimed:

1. A method for calculating a thickness t and a refractive index n of a liquid in a container, the method comprising:
providing an apparatus for measuring a quantity and optical parameters of the liquid in the container using optical low coherence reflectometry, the apparatus comprising:
a source arm comprising a low coherence light source;
a reference arm comprising a reference lens and a mirror, wherein a distance between the reference lens and the mirror is adjustable and measurable;
a test arm comprising a test lens;
a splitter for dividing an output of the source arm between the test arm and the reference arm;
a coupler for combining light reflected back into the reference arm and the test arm to create an interference signal; and
a device for detecting and analyzing the interference signal;

fixing the test lens in place with respect to the container with the test lens aimed through the container;
establishing a baseline optical path distance for light reflecting off of the container in an empty state by adjusting the distance between the reference lens and the mirror until a maximum interference signal is detected and determining a distance (X 0 ) between the reference lens and the mirror providing the maximum interference signal with the container in an empty state;
placing the liquid in the container or allowing the liquid to accumulate in the container;
establishing a first optical path distance for light reflecting directly back from the container by adjusting the distance between the reference lens and the mirror until a first strong maximum interference signal is detected and determining a distance (X 1 ) between the reference lens and the mirror providing the first strong maximum interference signal;
establishing a second optical path distance for light reflecting from the container after being passed through the liquid by adjusting the distance between the reference lens and the mirror until a second weak maximum interference signal is detected and determining a distance (X 2 ) between the reference lens and the mirror providing the second weak maximum interference signal;
determining a difference (ΔX 1 ) between the distance (X 1 ) between the reference lens and the mirror providing the first strong maximum interference signal and the distance (X 0 ) between the reference lens and the mirror providing the maximum interference signal with the container in an empty state;
determining a difference (ΔX 2 ) between the distance (X 2 ) between the reference lens and the mirror providing the second weak maximum interference signal and the distance (X 0 ) between the reference lens and the mirror providing the maximum interference signal with the container in an empty state; and
solving equations ΔX 1 =t·n−t and ΔX 2 =2t·n−t to determine the thickness t and the refractive index n of the liquid in the container.

2. The method as set forth in claim 1 wherein the source arm further comprises an isolator to prevent feedback from the reference arm and the test arm from entering the source arm.

3. The method as set forth in claim 1 wherein the low coherence light source further comprises an Erbium-doped fiber amplifier.

4. The method as set forth in claim 1 wherein the reference arm further comprises a phase modulator.

5. The method in claim 4 wherein the phase modulator comprises a function generator and the mirror is configured to be oscillated in accordance with the output of the function generator, with the function generator used to trigger the device for detecting and analyzing the interference signal.

6. The method as set forth in claim 1 wherein the test lens is a gradient-index lens.

7. The method as set forth in claim 1 wherein the device for detecting and analyzing the interference signal comprise a photodiode, an operational amplifier circuit, an analog-to-digital converter, and a computer.

8. The method as set forth in claim 1 wherein the source arm, the reference arm, the test arm, the splitter and the coupler comprise fiber optic components.

Assignees

• Univ Alberta

Inventors

• Fedosejevs Robert
• Utkin Ilya
• Sindhu Sunita
• Tsui Ying Yin

Classifications

• G01B9/0209 Primary

  Low-coherence interferometers · CPC title

• G01N21/45

  using interferometric methods; using Schlieren methods · CPC title

• G01B11/0625

  with measurement of absorption or reflection · CPC title

• G01B11/0675

  using interferometry · CPC title