Electric insulating oil inspection method, electric insulating oil treatment method, and oil-filled electric device maintenance method

Patent metadata

Field	Value
Publication number	US-9228992-B2
Application number	US-201013816261-A
Country	US
Kind code	B2
Filing date	Dec 13, 2010
Priority date	Dec 13, 2010
Publication date	Jan 5, 2016
Grant date	Jan 5, 2016

Abstract

The present invention relates to an electric insulating oil inspection method for determining whether or not an inhibitor-consuming substance is present in an electric insulating oil. The inhibitor-consuming substance is such a substance that causes to decrease over time a concentration of an inhibitor which is added to the electric insulating oil to inhibit copper sulfide from being generated on an insulating paper immersed in the electric insulating oil. The electric insulting oil inspection method includes steps of: preserving the electric insulating oil at a predetermined condition, measuring a concentration of the inhibitor, and determining that the inhibitor-consuming substance is present upon condition that a decrement of the concentration of the inhibitor relative to an initial concentration of the inhibitor becomes not less than a specified amount within a predetermined period.

First claim

The invention claimed is:

1. An electric insulating oil inspection method for determining whether or not an inhibitor-consuming substance is present in an electric insulating oil,
said inhibitor-consuming substance being such a substance that causes to decrease over time a concentration of an inhibitor which is added to said electric insulating oil to inhibit generation of copper sulfide on an insulating paper immersed in said electric insulating oil,
the electric insulating oil inspection method comprising:
a first step of preserving said electric insulating oil at a temperature of at least 40° C. but not higher than 60° C. and measuring the concentration of the inhibitor; and
a second step of determining that the inhibitor-consuming substance is present in the electric insulating oil upon condition that a decrement of the concentration of the inhibitor relative to an initial concentration thereof becomes not less than a specified amount within a predetermined period,
said inhibitor being a benzotriazole compound, and
the inhibitor-consuming substance being determined to be present at said second step upon condition that a decrease ratio of the concentration of the inhibitor in the electric insulating oil after 10 days from the start of inspection is greater than 10%.

2. The inspection method according to claim 1 , wherein said electric insulating oil is preserved at 40° C. at said first step.

3. The inspection method according to claim 1 , wherein said first step is performed under such a condition that only said electric insulating oil is present in a container without any other coexisting material.

4. An electric insulating oil treatment method in which whether or not an inhibitor-consuming substance is present in an electric insulating oil is preliminarily determined in accordance with the inspection method according to claim 1 , and a filtering treatment for removing the inhibitor-consuming substance from said electric insulating oil is performed upon condition that the inhibitor-consuming substance is determined to be present.

5. The electric insulating oil treatment method according to claim 4 , wherein said filtering treatment is a clay treatment.

6. An oil-filled electric device maintenance method employing the electric insulating oil treatment method according to claim 4 .

7. An electric insulating oil treatment method in which whether or not an inhibitor-consuming substance is present in an electric insulating oil is preliminarily determined in accordance with the inspection method according to claim 1 before adding to said electric insulating oil an inhibitor which inhibits generation of copper sulfide, a filtering treatment for removing the inhibitor-consuming substance from said electric insulating oil is performed upon condition that the inhibitor-consuming substance is determined to be present, and the inhibitor is added to said electric insulating oil after the filtering treatment.

Assignees

• Kato Fukutaro
• Nagao Eiichi
• Amimoto Tsuyoshi
• Toyama Satoru
• Mizuno Kota
• Mitsubishi Electric Corp

Inventors

• Kato Fukutaro
• Nagao Eiichi
• Amimoto Tsuyoshi
• Toyama Satoru
• Mizuno Kota

Classifications

• G01N33/287 Primary

  Sulfur content · CPC title

• G01N33/2835 Primary

  Specific substances contained in the oils or fuels · CPC title