Device for manufacturing aligned carbon nanotube assembly

Patent metadata

Field	Value
Publication number	US-9227171-B2
Application number	US-201013381034-A
Country	US
Kind code	B2
Filing date	Jun 29, 2010
Priority date	Jul 1, 2009
Publication date	Jan 5, 2016
Grant date	Jan 5, 2016

Abstract

Provided is a production apparatus ( 100 ) for continuously producing aligned carbon nanotube aggregates on a substrate supporting a catalyst while continuously transferring the substrate. The production apparatus ( 100 ) includes gas mixing prevention means ( 12, 13 ) for preventing gas present outside a growth furnace ( 3 a ) from flowing into the growth furnace ( 3 a ). The gas mixing prevention means ( 12, 13 ) includes a seal gas ejection section ( 12 b, 13 b ) so that the seal gas does not flow into the growth furnace through the openings of the growth furnace. The production apparatus prevents the outside air from flowing into the production apparatus, uniformly controls, within a range suitable to production of CNTs, a concentration distribution(s) and a flow rate distribution(s) of a raw material gas and/or a catalyst activation material on the substrate, and does not disturb gas flow as much as possible in the growth furnace.

First claim

The invention claimed is:

1. An apparatus for producing aligned carbon nanotube aggregates, the apparatus comprising:
a growth unit including a growth furnace for growing therein the aligned carbon nanotube aggregates on a substrate supporting a catalyst on a surface of the substrate; and
a first seal, the first seal comprising:
at least one seal gas ejection section that ejects seal gas along an opening plane of (i) an inlet or an outlet of the growth furnace or (ii) both the inlet and the outlet of the growth furnace; and
at least one exhaust section that exhausts the seal gas thus ejected so that the seal gas does not flow into the growth furnace.

2. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, wherein:
the growth unit includes a raw material gas ejection section for ejecting a raw material gas, and an exhaust hood for exhaustion of gas present in the growth furnace.

3. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, further comprising a formation unit including a formation furnace for causing the catalyst supported by the substrate to be surrounded by a reducing gas environment constituted by a reducing gas, and at least either the catalyst or the reducing gas is heated.

4. The apparatus as set forth in claim 3 for producing the aligned carbon nanotube aggregates, further comprising:
a second seal, the second seal comprising
at least one seal gas ejection section that ejects seal gas along an opening plane of (i) an inlet or an outlet of the formation furnace or (ii) both the inlet and the outlet of the formation furnace; and
at least one exhaust section that exhausts the seal gas thus ejected so that the seal gas does not flow into the formation furnace.

5. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, wherein:
the growth unit includes a catalyst activation material supplier for adding a catalyst activation material into the growth furnace.

6. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, wherein:
the at least one first seal gas ejection port is along an opening plane of the outlet of the growth furnace.

7. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, wherein:
the at least one seal gas ejection section of the first seal includes a catalyst activation material supplier for adding catalyst activation material.

8. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, wherein the growth unit is provided with a raw material gas injection section having a shower head including a plurality of injection holes facing a surface of the substrate on which the catalyst has been formed.

9. The apparatus as set forth in claim 3 for producing the aligned carbon nanotube aggregates, further comprising:
a first connection section between the growth unit and the formation unit,
wherein the first seal is in the first connection unit.

10. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, further comprising:
a cooling unit;
a second connection section between the growth unit and the cooling unit,
wherein the first seal is in the second connection unit.

11. The apparatus as set forth in claim 1 for producing the aligned carbon nanotube aggregates, further comprising:
a transfer unit moving the substrate supporting a catalyst through the apparatus, the transfer unit extending through openings in opposite sides of the apparatus.

12. An apparatus for producing aligned carbon nanotube aggregates, the apparatus comprising:
a growth unit including a growth furnace for growing therein the aligned carbon nanotube aggregates on a substrate supporting a catalyst on a surface of the substrate; and
a first seal, the first seal comprising:
at least one seal gas ejection section that ejects seal gas along an opening plane of (i) an inlet or an outlet of the growth furnace or (ii) both the inlet and the outlet of the growth furnace; and
at least one exhaust section that exhausts the seal gas thus ejected so that the seal gas does not flow into the growth furnace,

wherein the growth unit includes a raw material gas ejection section for ejecting a raw material gas, and an exhaust hood for exhaustion of gas present in the growth furnace, and
wherein the growth unit is provided with a raw material gas injection section having a shower head including a plurality of injection holes facing a surface of the substrate on which the catalyst has been formed.

Assignees

• Shibuya Akiyoshi
• Hata Kenji
• Yumura Motoo
• Zeon Corp
• Nat Inst Of Advanced Ind Scien

Inventors

• Shibuya Akiyoshi
• Hata Kenji
• Yumura Motoo

Classifications

• B01J15/005 Primary

  in the presence of catalytically active bodies, e.g. porous plates · CPC title

• B01J19/22 Primary

  in the form of endless belts · CPC title

• B01J19/0073

  Sealings (sealings for pressure vessels per se F16J15/00) · CPC title

• B01J2219/00159

  controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling · CPC title

• C01B31/024

  Chemistry & Metallurgy · mapped topic