Volatile compounds trap desorption device and method for desorbing volatile compounds from a trap

Patent metadata

Field	Value
Publication number	US-9222855-B2
Application number	US-201113820741-A
Country	US
Kind code	B2
Filing date	Sep 1, 2011
Priority date	Sep 6, 2010
Publication date	Dec 29, 2015
Grant date	Dec 29, 2015

Abstract

A method for restoring a volatile compound from a trapping means, wherein the method includes a flowing step wherein a carrier gas flows through the trapping means, at a controlled rate, by increasing the volume of a chamber located downstream of the trapping means is disclosed. The invention also relates to a device for implementing the method. The invention allows to faithfully restore the compounds that have been previously trapped and to faithfully restore the trapped odors.

First claim

What is claimed is:

1. A method for restoring a volatile compound that is trapped in a trapping means ( 8 ), wherein the method includes the steps of: flowing a carrier gas through the trapping means, at a controlled rate, to a chamber ( 30 ) of adjustable volume located downstream of the trapping means by increasing the volume of the chamber; and heating the trapping means during the flowing of the carrier gas therethrough to restore the volatile compound; wherein the heating is provided by moving heating means ( 10 ) from a first position remote from the trapping means to a second position close to the trapping means, with the heating means including an inertial element ( 13 ) therein that includes a first cut out portion ( 14 ) that surrounds at least a portion of the trapping means in the second position, and a thermal insulating material except at the cut out portion; and directing heat to the trapping means by radiation and conduction from the inertia material of the heating means.

2. The method of claim 1 , wherein the increase of the volume of the chamber includes a controlled deformation or controlled movement of a wall of the chamber.

3. The method of claim 1 , wherein the chamber comprises a cylinder ( 2 ) and a piston ( 3 ) and wherein the increase of the volume of the chamber includes a controlled movement of the piston in the cylinder.

4. The method of claim 1 , wherein the flowing step includes a first flowing sub-step during which the trapping means is not heated.

5. The method of claim 4 , wherein the flowing step includes a second flowing sub-step during which the trapping means is heated.

6. The method of claim 1 , wherein the carrier gas is a moist carrier gas.

7. The method of claim 1 , wherein the chamber is maintained at a predetermined temperature during the increasing of the volume of the chamber.

8. A device ( 1 ) for restoring a volatile compound that is trapped in a trapping means ( 8 ), wherein the device includes the heating means ( 10 ) and hardware means ( 2 , 3 , 4 , 5 , 6 , 7 , 9 , 10 , 20 , 21 , 22 ) software means for implementing the method according to claim 1 .

9. The device according to claim 8 , wherein the hardware means includes a chamber ( 30 ) and controlling means ( 20 , 21 , 22 ) for controlling the volume of the chamber.

10. The device according claim 8 , wherein the controlling means comprises an actuator ( 20 , 21 ) controlled by a logic processing unit ( 22 ), alone or included in a computer, with the actuator controlling deformation or movement of a wall of the chamber.

11. The device according to claim 10 , wherein the actuator includes a motor ( 20 ).

12. The device according to claim 9 , wherein the chamber includes a cylinder ( 2 ) and a piston ( 3 ).

13. The device according to claim 12 , wherein at least one surface of the cylinder or the piston is made of stainless steel that is passivated.

14. The device according to claim 8 , wherein the heating means is rotatably mounted on a means ( 6 ) for securing the trapping means or on an element ( 4 ) directly or indirectly secured to the means ( 6 ) for securing the trapping means.

15. The device of claim 12 wherein the trapping means is directly connected to the piston to limit travel distance of the restored compound from the trapping means to the chamber.

16. The method of claim 3 which further comprises directly connecting the trapping means to the piston to limit travel distance of the restored compound from the trapping means to the chamber.

17. The device of claim 15 wherein the trapping means includes securing means ( 6 , 7 ) on each end and the inertial element ( 13 ) includes second ( 15 ) and third ( 16 ) cut out portions that are larger than the first cut out portion for respectively surrounding the securing means ( 6 , 7 ), with each cut out portion being U-shaped.

18. The method of claim 16 which further comprises providing securing means ( 6 , 7 ) on each end of the trapping means and providing second ( 15 ) and third ( 16 ) cut out portions on the inertial element ( 13 ), wherein the second and third cut out portions are larger than the first cut out portion and respectively surround the securing means ( 6 , 7 ), with each cut out portion being U-shaped.

19. The device of claim 10 wherein the inertial element ( 13 ) comprises an electric resistor heater ( 19 ) and a temperature sensor ( 31 ) for controlling the resistor heater with each of the resistor heater and sensor operatively associated with the logic processing unit ( 22 ).

20. The method of claim 1 wherein the inertial element ( 13 ) comprises an electric resistor heater ( 19 ) and a temperature sensor ( 31 ) for controlling the resistor heater with each of the resistor heater and sensor operatively associated with a logic processing unit ( 22 ).

Assignees

• Chaintreau Alain
• Begnaud Frédéric
• Keller Urs
• Firmenich & Cie

Inventors

• Chaintreau Alain
• Begnaud Frédéric
• Keller Urs

Classifications

• B01J20/3458

  in the gas phase · CPC title

• G01N1/405

  by adsorption or absorption · CPC title

• B01D2259/40086

  by using a purge gas (B01D2259/4009 takes precedence) · CPC title

• G01N1/22 Primary

  in the gaseous state {(specially adapted for biological material G01N33/497; measuring breath flow A61B5/087)} · CPC title

• B01J20/3425

  of sorbents or filter aids comprising organic materials · CPC title