Ultrasensitive rapid antigen detection kit and detection method thereof
US-2024345078-A1 · Oct 17, 2024 · US
US9212979B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9212979-B2 |
| Application number | US-201414155429-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 15, 2014 |
| Priority date | Jan 15, 2014 |
| Publication date | Dec 15, 2015 |
| Grant date | Dec 15, 2015 |
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An automated headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry for the determination of four N-nitrosamines in groundwater samples is developed. Response surface methodology technique was employed to investigate the optimized extraction conditions of headspace solid-phase microextraction using CombiPAL autosampler. The method was applied to determine the N-nitrosamine concentrations in groundwater samples.
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The invention claimed is: 1. An automated headspace solid-phase microextraction gas chromatography-mass spectrometry method for determining nitrosamine concentration, comprising: mixing a nitrosamine-containing aqueous sample that has not been pretreated with one or more salts in a vial comprising an SPME fiber at a headspace portion above the unfiltered nitrosamine-containing aqueous sample in the vial; extracting a nitrosamine-containing analyte from the nitrosamine-containing…
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