Liquid crystal polymer pellet, liquid crystal polymer powder, liquid crystal polymer film, and method of producing same
US-2024208182-A1 · Jun 27, 2024 · US
US9114550B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9114550-B2 |
| Application number | US-201213629187-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 27, 2012 |
| Priority date | Feb 14, 2012 |
| Publication date | Aug 25, 2015 |
| Grant date | Aug 25, 2015 |
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In the process of forming a wood pulp fiber and thermoplastic polymer composition the step of decreasing the exit area of the mixing device to 40 to 60% of the cross-sectional area of the mixing device.
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The invention claimed is: 1. A method of making a composition, comprising: providing chemical wood pulp fibers in the form of particles and thermoplastic polymer to a mixing device, wherein for every 100 weight percent of material provided to the mixer, the pulp fibers comprise 65 to 90 weight percent of the material, mixing the fiber and the polymer in the mixing device to form a fiber/polymer blend in which substantially individual wood pulp fibers are dispersed within the polymer, wherein the exit area of the mixing device is 40 to 60% of the cross-sectional area of the mixing device, and thereafter forming the fiber/polymer blend into pellets. 2. The method of claim 1 wherein the thermoplastic polymer is selected from the group consisting of a biopolymer, polylactic acid, cellulose acetate, cellulose propionate, cellulose butyrate, a polycarbonate, polyethylene terephthalate, a polyolefin, polyethylene, high density polyethylene, low density polyethylene, linear low density polyethylene, polypropylene, polystyrene, a polystyrene copolymer, acrylonitrile-butadiene-styrene copolymer, a styrene block copolymer, polyvinyl chloride, and a recycled plastic. 3. The method of claim 1 wherein the mixing device has two intermeshing rotors. 4. The method of claim 1 wherein the step of forming the blend into pellets comprises further mixing the fiber/polymer blend in a second mixing device, wherein the second mixing device uses split flow to disperse the fibers in the polymer, and thereafter forming the blend into pellets. 5. The method of claim 4 wherein the wood pulp fibers are bleached chemical wood pulp fibers. 6. The method of claim 4 wherein the thermoplastic polymer is selected from the group consisting of a biopolymer, polylactic acid, cellulose acetate, cellulose propionate, cellulose butyrate, a polycarbonate, polyethylene terephthalate, a polyolefin, polyethylene, high density polyethylene, low density polyethylene, linear low density polyethylene, polypropylene, polystyrene, a polystyrene copolymer, acrylonitrile-butadiene-styrene copolymer, a styrene block copolymer, polyvinyl chloride, and a recycled plastic. 7. The method of claim 1 wherein the step of forming the blend into pellets comprises further mixing the fiber/polymer blend in a second mixing device, wherein the second mixing device has two intermeshing rotors, and thereafter forming the blend into pellets. 8. The method of claim 7 wherein the wood pulp fibers are bleached chemical wood pulp fibers. 9. The method of claim 8 wherein the thermoplastic polymer is selected from the group consisting of a biopolymer, polylactic acid, cellulose acetate, cellulose propionate, cellulose butyrate, a polycarbonate, polyethylene terephthalate, a polyolefin, polyethylene, high density polyethylene, low density polyethylene, linear low density polyethylene, polypropylene, polystyrene, a polystyrene copolymer, acrylonitrile-butadiene-styrene copolymer, a styrene block copolymer, polyvinyl chloride, and a recycled plastic. 10. The method of claim 1 wherein the fiber/polymer blend travels a distance from the mixing device to the exit and the cross section of the path of travel gradually diminishes between the mixing device and the exit. 11. A method of making a composition, comprising: providing thermoplastic polymer and particles consisting of chemical wood pulp fibers to a mixing device, wherein for every 100 weight percent of material provided to the mixer, the wood pulp fibers are 65 to 90 weight percent of the material, mixing the particles and the polymer in the mixing device to form a fiber/polymer blend in which the substantially individual chemical wood pulp fibers are dispersed within the polymer, urging the fiber/polymer blend from the mixing device through an exit having an area that is 40 to 60% of the cross-sectional area of the mixing device, and thereafter forming the fiber/polymer blend into pellets. 12. The method of claim 1 , wherein for every 100 weight percent of material provided to the mixing device, the wood pulp fibers are 75 to 90 weight percent of the material. 13. The method of claim 1 , wherein for every 100 weight percent of material provided to the mixing device, the wood pulp fibers are 80 to 90 weight percent of the material. 14. The method of claim 11 , wherein for every 100 weight percent of material provided to the mixing device, the wood pulp fibers are 75 to 90 weight percent of the material. 15. The method of claim 11 , wherein for every 100 weight percent of material provided to the mixing device, the wood pulp fibers are 80 to 90 weight percent of the material.
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