Apparatus for producing surface enhanced membrane

Patent metadata

Field	Value
Publication number	US-9108159-B2
Application number	US-87596510-A
Country	US
Kind code	B2
Filing date	Sep 3, 2010
Priority date	Jan 22, 2001
Publication date	Aug 18, 2015
Grant date	Aug 18, 2015

Abstract

A membrane having a refined surface as well as to a process and an apparatus for producing such a membrane, and which is useful, in particular, for rapid diagnostic tests for identifying specific analytes in liquid media.

First claim

The invention claimed is:

1. An apparatus for refining a surface of a membrane composed of cellulose produced by phase inversion in an evaporation process, said apparatus comprising:
at least one membrane drawing machine for producing a feedstock membrane by phase inversion in an evaporation process;
at least one membrane cleansing device comprising at least one wiper provided with a resilient wiper element or suction device for bringing at least one side of the feedstock membrane from which impurities such as filter dust are to be removed into contact with at least one cleansing agent or mechanical cleansing device, and
at least one membrane dryer;
wherein said membrane cleansing device is arranged between the membrane drawing machine and the membrane dryer at a position at which the feedstock membrane is in a partially-solidified state in which a fraction of solvent in the partially-solidified membrane is between 5-20% by weight of a fraction of solvent in a pre-casting feedstock solution, and
wherein the membrane cleansing device comprises a wiper roller with wiper elements arranged on an outer surface thereof, said wiper roller rotating in the direction in which the membrane is drawn, and at a speed greater than the speed at which the membrane is drawn.

2. An apparatus according to claim 1 , wherein the membrane cleansing device comprises at least one rinsing device for rinsing the side of the feedstock membrane from which impurities are to be removed, with a cleansing liquid comprising at least one cleansing agent.

3. An apparatus according to claim 2 , wherein a first rinsing device is arranged immediately downstream of the membrane drawing machine and a second rinsing device is arranged immediately upstream of the membrane dryer.

4. An apparatus according to claim 3 , wherein said first rinsing device comprises at least one nozzle for spraying a washing liquid on the side of the membrane from which impurities are to be removed.

5. An apparatus according to claim 3 , wherein said first and second rinsing devices each comprise a washing basin for holding a cleansing liquid, and guide rollers for transporting the membrane through the respective washing basins.

6. An apparatus according to claim 5 , wherein the washing basin of the second rinsing device contains a washing liquid, which, in turn, contains at least one additive.

7. An apparatus according to claim 6 , wherein the additive is a wetting agent.

8. An apparatus according to claim 1 , wherein each wiper comprises a wiper element having a width at least equal to the membrane and arranged on the resilient element so that when the membrane is moved relative to the wiper, the wiper element will sweep over the side of the membrane from which impurities are to be removed.

9. An apparatus according to claim 1 , wherein membrane cleansing device further comprises a support roller which rotates in the direction in which the membrane is drawn and at the speed at which the membrane is drawn, said support roller being arranged to form a nip with the wiper roller through which the membrane is guided.

10. An apparatus according to claim 8 , wherein each wiper element comprises a rubber wiper or a brush.

11. An apparatus according to claim 2 , wherein said rinsing device comprises a wash basin containing a cleansing liquid and at least one wiping element arranged above the wash basin to wipe cleansing liquid from the membrane emerging from the wash basin.

12. An apparatus for refining a surface of a membrane composed of cellulose produced by phase inversion in an evaporation process, said apparatus comprising:
at least one membrane drawing machine for producing a feedstock membrane by phase inversion in an evaporation process;
at least one membrane cleansing device comprising at least one wiper provided with a resilient wiper element or suction device for bringing at least one side of the feedstock membrane from which impurities such as filter dust are to be removed into contact with at least one cleansing agent or mechanical cleansing device, and
at least one membrane dryer;
wherein said membrane cleansing device is arranged between the membrane drawing machine and the membrane dryer at a position at which the feedstock membrane is in a partially-solidified state in which a fraction of solvent in the partially-solidified membrane is between 5-20% by weight of a fraction of solvent in a pre-casting feedstock solution,
wherein each wiper comprises a wiper element having a width at least equal to the membrane and arranged on the resilient element so that when the membrane is moved relative to the wiper, the wiper element will sweep over the side of the membrane from which impurities are to be removed, and
wherein said wiper elements are provided with nozzles for spraying a rinsing liquid onto the wiper elements.

Assignees

• Beer Hans
• Froese Klaus
• Knoechelmann Lothar
• Piechocki Duane B
• Sartorius Stedim Biotech Gmbh

Inventors

• Beer Hans
• Froese Klaus
• Knoechelmann Lothar
• Piechocki Duane B

Classifications

• B01D69/02

  characterised by their properties · CPC title

• Y10T436/255

  including use of a solid sorbent, semipermeable membrane, or liquid extraction · CPC title

• B01D71/20

  Esters of inorganic acids, e.g. cellulose nitrate · CPC title

• Y10T436/25125

  Digestion or removing interfering materials · CPC title

• B01D2323/12

  Specific ratios of components used · CPC title