Processes for Producing Acetic Acid
US-2015376105-A1 · Dec 31, 2015 · US
US9063045B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9063045-B2 |
| Application number | US-201313958810-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 5, 2013 |
| Priority date | Feb 28, 2008 |
| Publication date | Jun 23, 2015 |
| Grant date | Jun 23, 2015 |
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A method for pretreating and extracting a liquid sample by sorbing an aqueous liquid sample, including an organic analyte and an acid or a base, in a solid sorbent material, and at least partially neutralizing the acid or base by reaction with neutralizing ions retained on a support surface, and contacting the liquid sample-sorbed sorbent material at elevated temperature and pressure with an organic solvent to extract the analyte into said solvent, preferably in a vessel having an extraction chamber with a zirconium metal interior surface.
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What is claimed is: 1. A method of separating an organic analyte from a base in a sample comprising: a) sorbing a sample in a solid sorbent material having a surface comprising cationic moieties, wherein the sample includes an organic analyte and a base and wherein the cationic moieties react with the base; and b) contacting the sample-sorbed sorbent material with an organic solvent to extract the organic analyte; c) collecting the organic solvent with the extracted analyte, t…
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