Graphene composite, method for producing graphene composite and electrode for lithium ion battery containing graphene composite
US-2016351908-A1 · Dec 1, 2016 · US
US9051275B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9051275-B2 |
| Application number | US-201113577078-A |
| Country | US |
| Kind code | B2 |
| Filing date | Feb 4, 2011 |
| Priority date | Feb 4, 2010 |
| Publication date | Jun 9, 2015 |
| Grant date | Jun 9, 2015 |
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The present invention relates to polymorphs and solvates of the hydrochloride salt of 4-[2-[[5-methyl-1-(2-naphthalenyl)-1H-pyrazol-3-yl]oxy]ethyl]morpholine (P027), processes for their preparation, and to pharmaceutical compositions comprising them.
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The invention claimed is: 1. A solid polymorphic or solvated form of the hydrochloride salt of 4-[2-[[5-methyl-1-(2-naphthalenyl)-1H-pyrazol-3-yl]oxy]ethyl]morpholine selected from the group consisting of: a) a polymorphic phase I form having a X-ray powder diffraction pattern showing characteristic peaks at a reflection angle [2θ in degrees] of about 5.9, 8.1, 11.3, 11.7, 14.2, 15.1, 15.8, 16.3, 16.8, 17.8, 18.1, 18.6, 19.8, 20.9, 21.9, 22.8, 23.0, 23.2, 23.6, 23.9, 24.3, 25.0, 2…
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