Method of preparing aromatic compounds from lignin
US-10081644-B2 · Sep 25, 2018 · US
US9045397B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9045397-B2 |
| Application number | US-201114365676-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 20, 2011 |
| Priority date | Dec 20, 2011 |
| Publication date | Jun 2, 2015 |
| Grant date | Jun 2, 2015 |
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Described herein are high yield methods for making magnolol analogs which are 5,5′-dialkyl-bi-phenyl-2,2′-diols.
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The invention claimed is: 1. A method for making 5,5′-dialkyl-biphenyl-2,2′-diols, comprising the following steps: (i) methylating biphenyl-2,2′-diol using dimethyl sulfate, to obtain 2,2′-dimethoxy-biphenyl; (ii) acylating the 2,2′-dimethoxy-biphenyl with an alkionyl chloride to obtain 2,2′-dimethoxy-5,5′-dialkionyl-biphenyl; (iii) reducing the 2,2′-dimethoxy-5,5′-dialkionyl-biphenyl to obtain 2,2′-dimethoxy-5,5′-dialkyl-biphenyl; (iv) demethylating the 2,2′-dimethoxy-5,5′-…
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
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