Geothermal energization of a non-combustion chemical reactor and associated systems and methods
US-9222704-B2 · Dec 29, 2015 · US
US9045347B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9045347-B2 |
| Application number | US-201113037151-A |
| Country | US |
| Kind code | B2 |
| Filing date | Feb 28, 2011 |
| Priority date | Feb 26, 2010 |
| Publication date | Jun 2, 2015 |
| Grant date | Jun 2, 2015 |
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A novel polycrystalline stoichiometric fine SiC fiber substantially free of impurities is produced using a novel pre-ceramic polymer. The pre-ceramic polymer is prepared by reacting a mixture of chlorodisilane, boron trichloride, and a vinyl chlorodisilane with an excess of hexamethyldisilazane to form the pre-ceramic polymer resin, which may then be melt-spun, cured, pyrolyzed and heat-treated to obtain the finished SiC fiber. The manufacturing process for the production of the fine SiC ceramic fiber allows for flexibility with respect to cross-linking, in that low-cost thermal treatments may replace more complex methods, while obtaining fibers with improved materials properties as compared to currently available SiC fibers.
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What is claimed is: 1. A method comprising: reacting a mixture of chlorodisilane (CDS), boron trichloride, and a vinyl chlorodisilane with hexamethyldisilazane (HMDS) to form a pre-ceramic polymer resin. 2. The method of claim 1 , wherein the mixture further comprises a compound selected from the group consisting of 1,1,3,3, tetraphenyldisilazane and 1,3 divinyltetramethyldisilazane, in the range of 5 to 35 percent by weight. 3. The metho…
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
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