High-temperature high-entropy alloy with light weight and high strength in as-cast state and preparation method thereof
US-2024410035-A1 · Dec 12, 2024 · US
US9039849B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9039849-B2 |
| Application number | US-200913394195-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 30, 2009 |
| Priority date | Sep 7, 2009 |
| Publication date | May 26, 2015 |
| Grant date | May 26, 2015 |
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Provided is a method of preparing a nanocrystalline titanium alloy at low strain to have better strength. The present invention is characterized in that an initial microstructure is induced as martensites having a fine layered structure, and then a nanocrystalline titanium alloy is prepared at low strain by optimizing process variables through observation of the effects of strain, strain rate, and deformation temperature on the changes in the microstructure.
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The invention claimed is: 1. A method of preparing a nanocrystalline titanium alloy, the method comprising; segmenting a martensite structure haying a layered structure into a fine equiaxed structure having a size range of 200 nm to 400 nm by rolling under conditions that a deformation temperature ranges from 575° C. to 625° C., a strain rate ranges from 0.07 to 0.13 s −1 , and a strain ranges from 0.9 to 1.8, wherein a dynamic spheroidization is generated when the layered structure of the martensite structure is entirely segmented into the fine equiaxed structure. 2. The method of claim 1 , wherein the deformation temperature is 600° C., the strain rate is 0.1 s −1 , and the strain is 1.4. 3. The method of claim 1 , wherein the martensite structure is obtained from an initial microstructure of a Ti-13Nb-13Zr alloy by water quenching the initial microstructure after being maintained at 800° C. for 30 minutes.
Alloys based on titanium · CPC title
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