Method for evaluating polymer material

Patent metadata

Field	Value
Publication number	US-9000367-B2
Application number	US-201213982616-A
Country	US
Kind code	B2
Filing date	Feb 8, 2012
Priority date	Feb 8, 2011
Publication date	Apr 7, 2015
Grant date	Apr 7, 2015

Abstract

Provided is a method for evaluating a polymer material, wherein the state of dispersion of a filler in a polymer material can be quickly and quantitatively evaluated.
The method for evaluating a polymer material which is a polymer material containing the polymer compound and the filler and of which at least an upper surface is a flat surface. The polymer material 1 is cut in a direction at an angle α of 1 to 60° with respect to the surface of the polymer material using a focused ion beam (FIB) 10 , and a smooth surface 1 A of the polymer material, formed by the cutting, is then photographed in a direction perpendicular to the smooth surface.

First claim

The invention claimed is:

1. A method for evaluating a polymer material containing a polymer compound and a filler, of which at least an upper surface is a flat surface, the method comprising:
cutting the upper surface of the polymer material in a direction at an angle of 1 to 60° with respect to the upper surface of the polymer material using a focused ion beam; and then photographing a smooth surface of the polymer material, formed by the cutting, in a direction perpendicular to the smooth surface, and
wherein the filler is at least one selected from the group consisting of silicas, carbon blacks, and inorganic compounds represented by the following formula (I):
m M. x SiO y.z H 2 O  (I)

(wherein M is at least one selected from metals selected from the group consisting of aluminum, magnesium, titanium, calcium and zirconium, oxides or hydroxides of the metals and hydrates thereof, or carbonates of the metals; and m, x, y, and z are an integer of 1 to 5, an integer of 0 to 10, an integer of 2 to 5, and an integer of 0 to 10, respectively).

2. The method for evaluating a polymer material according to claim 1 , wherein the smooth surface of the polymer material is photographed using a scanning electron microscope.

3. The method for evaluating a polymer material according to claim 2 , wherein an image obtained by photographing the smooth surface of the polymer material is converted into a binarized image of a polymer compound section and a filler section, and the state of dispersion of the filler in the polymer material is evaluated based on the obtained binarized image.

4. The method for evaluating a polymer material according to claim 1 , wherein an image obtained by photographing the smooth surface of the polymer material is converted into a binarized image of a polymer compound section and a filler section, and the state of dispersion of the filler in the polymer material is evaluated based on the obtained binarized image.

Assignees

• Nakamura Satoshi
• KUROTANI Yuji
• Tanabe Tatsuro
• Igarashi Takaaki
• Bridgestone Corp

Inventors

• Nakamura Satoshi
• KUROTANI Yuji
• Tanabe Tatsuro
• Igarashi Takaaki

Classifications

• G01N1/286 Primary

  involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising (microtomes G01N1/06; pulverising in general B02C; mixing in general B01F) · CPC title

• G01N33/442

  Resins; Plastics · CPC title

• G01N23/00 Primary

  Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 · CPC title

• G01N23/225

  using electron or ion · CPC title