Method for producing carrier for electrode catalyst, precursor of carrier for electrode catalyst, and carrier for electrode catalyst, comprising same
US-12057587-B2 · Aug 6, 2024 · US
US8999599B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8999599-B2 |
| Application number | US-201213812233-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 17, 2012 |
| Priority date | Jul 19, 2011 |
| Publication date | Apr 7, 2015 |
| Grant date | Apr 7, 2015 |
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A method of fabricating a membrane electrode assembly, comprising: obtaining a mixture by mixing and kneading electrically conductive particles, a polymer resin, a surfactant, and a dispersion solvent (S 1 ); obtaining a sheet-like mixture by rolling out and shaping the mixture (S 2 ); obtaining a carbon sheet by heat-treating the sheet-like mixture at a first heat treatment temperature such that the surfactant and the dispersion solvent are removed from the sheet-like mixture (S 3 ); obtaining a dispersion liquid by mixing electrically conductive particles, a polymer resin, a surfactant, and a dispersion solvent (S 4 ); forming, on the carbon sheet, a dispersion liquid layer thinner than the carbon sheet by forming and drying a coating of the dispersion liquid on the carbon sheet (S 5 ); obtaining a gas diffusion layer in which a carbon layer is formed on the carbon sheet, by heat-treating the carbon sheet on which the dispersion liquid layer is formed at a second heat treatment temperature lower than the first heat treatment temperature such that the surfactant and the dispersion solvent are removed from the dispersion liquid layer (S 6 ); and stacking a catalyst layer and an electrolyte membrane in said order on the carbon layer (S 7 ).
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The invention claimed is: 1. A method of fabricating a membrane electrode assembly, the method comprising: obtaining a mixture by mixing first electrically conductive particles, a first polymer resin, a first surfactant, and a first dispersion solvent; obtaining a sheet-like mixture by shaping the mixture; obtaining a carbon sheet by heat-treating the sheet-like mixture at a first heat treatment temperature; obtaining a dispersion liquid by mixing second electrically conduct…
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