Single-crystal diamond and method of manufacturing the same
US-2024175167-A1 · May 30, 2024 · US
US8992877B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8992877-B2 |
| Application number | US-93305909-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 18, 2009 |
| Priority date | Jun 18, 2008 |
| Publication date | Mar 31, 2015 |
| Grant date | Mar 31, 2015 |
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A method of forming mono-crystalline diamond by chemical vapor deposition, the method comprising the steps of: (a) providing at least one diamond seed; (b) exposing the seed to conditions for growing diamond by chemical vapor deposition, including supplying reaction gases that include a carbon-containing gas and hydrogen for growing diamond and include a nitrogen-containing gas; and (c) controlling the quantity of nitrogen-containing gas relative to other gases in the reaction gases such that diamond is caused to grow by step-growth with defect free steps without inclusions. The nitrogen is present in the range of 0.0001 to 0.02 vol %. Diborane can also be present in a range of from 0.00002 to 0.002 vol %. The carbon-containing gas can be methane.
Opening claim text (preview).
The invention claimed is: 1. A method of forming mono-crystalline gem grade diamond by chemical vapour deposition, the method comprising the steps of: (a) providing at least one diamond seed; (b) exposing the seed to conditions for growing diamond by chemical vapour deposition, including supplying reaction gases that include a carbon-containing gas for growing diamond and include a nitrogen-containing gas; and (c) controlling the quantity of nitrogen-containing gas relative to…
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