Methods and compositions for increased thermoelectric oxide ceramic performance
US-2024132412-A1 · Apr 25, 2024 · US
US8992808B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8992808-B2 |
| Application number | US-201113220887-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 30, 2011 |
| Priority date | Jan 27, 2011 |
| Publication date | Mar 31, 2015 |
| Grant date | Mar 31, 2015 |
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The present invention relates to a method of manufacturing a porous pre-sintered granule for a sintered reaction-bonded silicon nitride, to which a pressure forming technology can be applied to obtain a porous sintered reaction-bonded silicon nitride having high porosity and having a structure in which macropores and micropores coexist with each other, and to a porous pre-sintered granule manufactured by the method. The method includes the steps of: granulating a raw material comprising silicon and sintering additives including yttrium, aluminum and at least one alkali earth metal compound; and pre-sintering the granulated raw material at a temperature of 1300˜1375° C. under an inert atmosphere. According to the present invention, a porous pre-sintered granule for porous sintered reaction-bonded silicon nitride, which can increase the air permeability and trapping efficiency by controlling the size of a pore channel such that macropores and micropores coexist, can be manufactured.
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What is claimed is: 1. A method of manufacturing a porous sintered reaction-bonded silicon nitride, comprising the steps of: granulating a raw material comprising silicon and sintering additive including yttrium, aluminum, and at least one alkali earth metal compound; pre-sintering the granulated raw material at a temperature of 1300˜1375° C. under an inert atmosphere to prepare porous granules; forming a compact with the porous granules; nitriding the compact under a nitrid…
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
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