Method for preparing organochlorosilanes
US-2022242887-A1 · Aug 4, 2022 · US
US8962877B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8962877-B2 |
| Application number | US-201013499707-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 28, 2010 |
| Priority date | Oct 16, 2009 |
| Publication date | Feb 24, 2015 |
| Grant date | Feb 24, 2015 |
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The invention pertains to a process for the preparation of organohalosilanes. The process comprises contacting a first finely-divided silicon comprising from 0.08 to 0.25% (w/w) of aluminum with an organohalide in a reactor at a temperature of from 250 to 350° C. in the presence of a Direct Process catalyst comprising copper, and a promotor; and introducing a second finely-divided silicon into the reactor comprising from 0.001 to <0.10% (w/w) of aluminum into the reactor as needed in an amount sufficient to maintain an aluminum concentration of from 0.08 to 0.2% (w/w), based on a weight of unreacted silicon and aluminum.
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We claim: 1. A method of preparing organohalosilanes, the method comprising: (i) contacting a first finely-divided silicon comprising from 0.08 to 0.25% (w/w) of aluminum with an organohalide in a reactor at a temperature of from 250 to 350° C. in the presence of a Direct Process catalyst comprising copper, and a promotor; and (ii) introducing a second finely-divided silicon comprising from 0.001 to<0.10% (w/w) of aluminum into the reactor as needed in an amount sufficient to ma…
Chemistry & Metallurgy · mapped topic
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