Compound for androgen receptor degradation, and pharmaceutical use thereof
US-2024383877-A1 · Nov 21, 2024 · US
US8961809B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8961809-B2 |
| Application number | US-201313842898-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 15, 2013 |
| Priority date | Jan 21, 2011 |
| Publication date | Feb 24, 2015 |
| Grant date | Feb 24, 2015 |
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A method of forming an electrolyte solution involves combining ammonium tetrafluoroborate and spiro-bi-pyrrolidinium bromide in a liquid solvent to form spiro-bi-pyrrolidinium tetrafluoroborate and an ammonium halide. The ammonium halide precipitate is removed from the solvent to form an electrolyte solution. The reactants can be added step-wise to the solvent, and the method can include using a stoichiometric excess of the ammonium tetrafluoroborate to form a substantially halide ion-free electrolyte solution.
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What is claimed is: 1. A method of forming an electrolyte solution comprising: combining ammonium tetrafluoroborate and spiro-bi-pyrrolidinium bromide in a liquid solvent to form spiro-bi-pyrrolidinium tetrafluoroborate and ammonium bromide; and removing the ammonium bromide from the solvent to form an electrolyte solution comprising spiro-bi-pyrrolidinium tetrafluoroborate. 2. The method according to claim 1 , wherein a molar ratio of ammonium tetrafluoro…
Electricity · mapped topic
Electricity · mapped topic
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